Method for preparing nanometer titanium dioxide through low temperature water steaming treatment
A technology of nano-titanium dioxide and water steaming, which is applied in the direction of titanium dioxide, chemical instruments and methods, titanium oxide/hydroxide, etc., can solve the problems of environmental protection, human health, unfavorable batch production, and complicated preparation process, so as to reduce fire hazards, The effect of low catalytic activity and high catalytic activity
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Embodiment 1
[0040] Under the state of vigorous stirring in a 30°C water bath at normal pressure, the mixed solution of tetrabutyl titanate and glacial acetic acid was added dropwise to the aqueous acetic acid solution, and the pH of the aqueous solution was controlled to be 2-3. The molar ratio of tetrabutyl titanate, deionized water, chelating agent and catalyst is 1:200:5:3. After the dropwise addition was completed, stirring was continued for 2 h. Static to aging for 48h, TiO with blue light is obtained 2 transparent sol. Then the aged nano-TiO 2 The sol was put into a glass watch glass, and dried in a steam system at 100°C under normal pressure for 8 hours to obtain nano-TiO 2 Powder.
[0041] Its XRD patterns and performance indicators are shown in image 3 and Table 2.
[0042] Table 2 TiO prepared under atmospheric pressure steam system 2 Powder properties
[0043]
Embodiment 3
[0045] Under the state of vigorous stirring in a 30°C water bath at normal pressure, the mixed solution of tetrabutyl titanate and glacial acetic acid was added dropwise to the aqueous acetic acid solution, and the pH of the aqueous solution was controlled to be 2-3. The molar ratio of tetrabutyl titanate, deionized water, chelating agent and catalyst is 1:190:5:5. After the dropwise addition was completed, stirring was continued for 2 h. Static to aging for 48h, TiO with blue light is obtained 2 transparent sol. Then the aged nano-TiO 2 The sol was put into a glass watch glass and dried in a steam system at 0.18MPa and 130°C for 6h to obtain TiO 2 Powder. Its XRD see Figure 4 , and the performance is shown in Table 3 below.
[0046] Table 3 TiO prepared under high pressure steam system 2 Powder properties
[0047]
[0048] It can be seen that the nano-TiO obtained by the high-pressure steam drying system 2 The powder has good photocatalytic activity, and the 5mg / ...
Embodiment 4
[0050] A method for preparing nano-titanium dioxide by steaming at low temperature, the process flow is as follows figure 1 shown, including the following steps:
[0051] (1) Mix tetrabutyl titanate and glacial acetic acid evenly to obtain a yellow solution.
[0052] (2) Mix deionized water and glacial acetic acid, pour it into a three-necked flask, put it in a constant temperature water bath at 30°C, and slowly add the yellow solution in step (1) to the aqueous acetic acid solution under stirring with an electric stirrer After dropping, continue to stir vigorously for 2 hours, and after aging for 48 hours, a transparent nano-TiO2 aqueous sol with blue light is obtained. The molar ratio of the tetrabutyl titanate, deionized water, chelating agent and catalyst is 1:200:5:3.
[0053] (3) Select the soft base material cotton fabric as the base material, immerse the aged nano-TiO 2 In the hydrosol, immerse in a water steaming system at normal pressure 100°C for 8 hours, wash an...
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