Efficient method for separating solid residue and product in lignocellulose fermented mash

A technology for lignocellulose and solid residues, applied in the field of lignocellulose, can solve the problems of accelerated equipment loss, expensive equipment, high centrifugal energy consumption, etc., and achieve the effects of avoiding economic benefits, reducing energy consumption, and improving production processes

Inactive Publication Date: 2013-05-15
EAST CHINA UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the small particle size of these particles, traditional separation methods such as distillation, centrifugation, plate and frame filter press, etc. are difficult to work
For example, in the process of distillation, due to the existence of a large amount of solid residue, the pipeline will be blocked and the bottom of the kettle will be severely coked, which will greatly reduce the separation efficiency and service life of the distillation tower, and accelerate the loss of equipment; centrifugal energy consumption is large, and the equipment is expensive ;During the plate and frame filter press process, the viscosity of the fermentation liquid is extremely high, and the diameter of the solid particles is very small, which can easily cause the filter cloth to be blocked and effectively separate the solid residue from the product.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Prepare 10g / l chitosan acetic acid solution; weigh lignocellulose lactic acid mash with 25% solid content, measure its water content as 72.75%, and lactic acid concentration as 67.28g / l; measure 100ml lignocellulose lactic acid fermentation with a graduated cylinder Dash, then weigh its mass 110.51g with an electronic balance, and pour it into a 150ml beaker; at room temperature, add 8ml of 10g / l chitosan acetic acid solution, and stir with a glass rod for 5min to make it evenly mixed; Transfer all the mixed solution into the Buchner funnel with a single layer of qualitative filter paper, connect a graduated suction filter bottle under the Buchner funnel, turn on the circulating vacuum pump to make the pressure reach 0.1Mpa, and filter for 25 minutes to obtain the volume of lactic acid serum 62.9ml, the measured lactic acid concentration was 59.71g / l. The calculated recovery rate of lactic acid was 68.99%.

[0026] Lactic acid recovery calculation method:

[0027] Lac...

Embodiment 2

[0030] Prepare 10g / l chitosan acetic acid solution; weigh the lignocellulose lactic acid fermentation mash with 25% solid content, measure its water content to be 73.13%, and the lactic acid concentration to be 72.27g / l; measure 200ml lignocellulose with a graduated cylinder Lactic acid fermented mash, and weighed 224.6g with an electronic scale; pour it into a 250ml beaker, add 16ml of 10g / l chitosan acetic acid solution, stir with a glass rod for 5min to make it evenly mixed; completely transfer it to the press Put it in the bag, put it into the press machine and press it under the pressure of 10Mpa for 2min. After the pressing, take out the press bag, measure the residual solid mass of 37.51g after pressing, and measure its water content to 51.11%. The recovery rate of lactic acid was 76.12%.

[0031] Lactic acid recovery calculation method:

[0032] Lactic acid recovery rate = (mass of cellulose lactic acid fermented mash before pressing (g) × water content (%) of cellulo...

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PUM

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Abstract

The invention relates to an efficient method for separating solid residue and products in lignocellulose fermented mash. The method comprises the specific steps of: (1) preparing a flocculant solution; (2) evenly mixing the lignocellulose fermented mash with a flocculant solution, and stirring for 5 min to fully contact the flocculant with the lignocellulose solid; and (3) conducting a solid-liquid separation on the mixed fermented mash by using a mill or a vacuum filtration device, so as to obtain a clear liquid containing fermentation products and lignocellulose solid residue. The invention has wide raw material resources, greatly reduces energy consumption of the solid-liquid separation in the condition of ensuring yield of effective products in the lignocellulose fermented mash, further improves the production process of fuel ethanol and bulk chemicals from biotransformation lignocellulose, and provides technical reserve for industrialization of lignocellulose biorefinery.

Description

【Technical field】 [0001] The invention relates to the technical field of lignocellulose, in particular to a method for efficiently separating solid residues and products in lignocellulose fermentation mash. 【Background technique】 [0002] The use of abundant and renewable lignocellulosic biomass to produce liquid fuels and bulk chemicals can effectively alleviate human dependence on fossil resources and improve the increasingly serious environmental pollution and greenhouse effect. At present, it has become the research and development focus and priority development strategy of major countries. [0003] When bioconverting lignocellulosic raw materials to produce biofuels and bio-based chemicals, the simultaneous saccharification and fermentation process (Simultaneous saccharification and fermentation, SSF) is generally adopted, which can reduce the inhibition of cellulase by sugar and improve the production efficiency of cellulosic raw materials. The conversion rate; at the...

Claims

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Application Information

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IPC IPC(8): B01D37/03C08H7/00C07C59/08C07C51/42
Inventor 鲍杰包艳文张建
Owner EAST CHINA UNIV OF SCI & TECH
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