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PVB (polyvinyl butyral) film having heat-insulating property and preparation method thereof

A membrane and performance technology, applied in the field of PVB membrane and its preparation, can solve the problems of ITO nano powder agglomeration, etc., and achieve the effect of solving agglomeration, good heat insulation effect and high blocking rate

Active Publication Date: 2013-04-17
吴莉
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The invention provides a PVB diaphragm with thermal insulation performance and a preparation method thereof, which can effectively solve the problem of agglomeration when ITO nanometer powder is added, and the process for preparing the PVB diaphragm is simple and easy to use; The laminated glass has a good heat insulation effect, and has a high blocking rate for mid-infrared rays with a wavelength of 1500-2100nm.

Method used

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  • PVB (polyvinyl butyral) film having heat-insulating property and preparation method thereof

Examples

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Effect test

Embodiment 1

[0042] Take methanol: 84g, PVB resin powder: 5g, ITO nano-powder: 11g, add PVB resin powder into methanol to dissolve, then add ITO nano-powder and grind on a ball mill for 3 hours to prepare nano-ITO emulsion.

Embodiment 2

[0044] Take ethanol: 85g, PVB resin powder: 10g, ITO nano-powder: 5g, add PVB resin powder to ethanol to dissolve, then add ITO nano-powder and grind on a ball mill for 4 hours to prepare nano-ITO emulsion.

Embodiment 3

[0046] Get ethyl acetate: 70g, PVB resin powder: 15g, ITO nano-powder: 15g, add PVB resin powder in ethyl acetate and dissolve, then add ITO nano-powder and grind on a ball mill for 5 hours to make a nano-ITO emulsion.

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Abstract

The invention provides a PVB (polyvinyl butyral) film having heat-insulating property, which comprises the following components in percentage by mass: 0.1-1% of ITO (indium tin oxide) nano emulsion, 19-40% of plasticizer, 59-80% of PVB resin powder, 0.1-2% of antioxidant and 0.05-1% of ultraviolet absorbent, wherein the ITO nano emulsion comprises the following components in percentage by mass: 65-90% of organic solvent, 5-20% of PVB resin powder and 5-15% of ITO nano powder. The invention also relates to a preparation method of the PVB film having heat-insulating property, which comprises the following steps: dissolving a small amount of PVB in organic solvent, adding a right amount of ITO powder, and repeatedly milling to a nano level with a ball mill, thus obtaining a nano emulsion; proportionally mixing the nano emulsion with the plasticizer, and adding into the PVB resin powder; and plastifying in a plastic extruding machine, and performing film formation through a mold, thus obtaining the PVB film. Thus, the invention effectively solves the aggregation problem.

Description

technical field [0001] The invention relates to a PVB diaphragm with thermal insulation performance and a preparation method thereof. Background technique [0002] Since the introduction of polyvinyl butyral (hereinafter referred to as PVB) film laminated glass in the United States in 1935 and its use in automobiles by law in 1938, especially since 1964, for the safety of passengers, high penetration glass has been gradually developed. Li's PVB film laminated glass has been used as a standard in many countries. However, with the development of the times, the requirements of passengers have gradually increased, so it is necessary to develop PVB membranes with special functions to produce laminated glass, among which the heat insulation function is representative. [0003] In order to pursue a sense of openness, a large area of ​​glass is used. At the same time, taking into account the heat input and the load ratio of the air conditioner, combining comfort and environmental p...

Claims

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Application Information

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IPC IPC(8): C08L29/14C08K13/06C08K9/04C08K3/22C08K5/11
Inventor 卢士海殷发强朱仕惠蒋愿何佳文
Owner 吴莉
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