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Method for preparing high temperature resistant nickel base alloy

A nickel-based alloy, high-temperature-resistant technology, applied in the field of alloy metals, can solve problems such as large difference in initial melting temperature and plasticity, poor plasticity and oxidation resistance, and limit the application of alloys, and achieve high-temperature strength, good high-temperature durability, The effect of improving tissue stability

Inactive Publication Date: 2012-12-05
瑞安市劲力机械制造有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Although many nickel-based superalloys for aero-engines have been developed in China, such as K403, K405, K441 and K417G alloys, the biggest disadvantage of these alloys is that the initial melting temperature and plasticity are quite different from those of cobalt-based superalloys. application of these alloys
Although intermetallic compounds have the characteristics of low specific gravity and high strength, their use is limited due to their poor plasticity and oxidation resistance.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A method for preparing a high-temperature resistant nickel-based alloy, the nickel-based alloy is composed of the following components in weight percentage: Cr: 26.0%, Co: 5.7%, Mo: 8.2%, W: 2.8%, V: 0.4% , Ta: 4.2%, Al: 5.6%, Ti: 1.7%, Nb: 2.1%, B: 0.006%, 0.1≤Cu≤0.4, 0<C≤0.08, 0<Si≤0.3, 0<Mn≤0.5, The balance is Ni, and the preparation method is as follows: after batching according to the above alloy components, smelting is carried out, the vacuum is controlled to reach 0.01Pa, and the melting power is kept constant for 25 minutes after all the raw materials are melted; Refining at ℃ for 6 minutes, adjusting the composition to meet the requirements; then adjusting to 1620℃ and pouring into ingots; then heat treatment, first heating the ingot to 1250℃, keeping it for 5 hours, then air cooling to room temperature; then heating to 1140℃, and keeping it for 5 hours , air-cooled to room temperature; then heated to 1050 ℃, heat preservation 36h, air-cooled to room temperatur...

Embodiment 2

[0022] A method for preparing a high-temperature resistant nickel-based alloy, the nickel-based alloy is composed of the following components in terms of weight percentage: Cr: 28.0%, Co: 5.3%, Mo: 8.6%, W: 2.4%, V: 0.6% , Ta: 3.8%, Al: 6.0%, Ti: 1.3%, Nb: 2.5%, B: 0.004%, 0.1≤Cu≤0.4, 0<C≤0.08, 0<Si≤0.3, 0<Mn≤0.5, The balance is Ni, and the preparation method is as follows: after batching according to the above alloy components, smelting is carried out, and the vacuum degree is controlled to reach 0.1Pa. After all the raw materials are melted, the melting power is kept unchanged for 15 minutes; the vacuum degree is increased to 0.01Pa. Refining at ℃ for 8 minutes, adjusting the composition to meet the requirements; then adjusting to 1600℃ and pouring into ingots; then heat treatment, first heating the ingot to 1270℃, keeping it for 3 hours, then air cooling to room temperature; then heating to 1160℃, and keeping it for 3 hours , air-cooled to room temperature; then heated to 1...

Embodiment 3

[0024] A method for preparing a high-temperature resistant nickel-based alloy, the nickel-based alloy is composed of the following components in terms of weight percentage: Cr: 27.0%, Co: 5.5%, Mo: 8.4%, W: 2.6%, V: 0.5% , Ta: 4.0%, Al: 5.8%, Ti: 1.5%, Nb: 2.3%, B: 0.005%, 0.1≤Cu≤0.4, 0<C≤0.08, 0<Si≤0.3, 0<Mn≤0.5, The balance is Ni, and the preparation method is as follows: after batching according to the above alloy components, smelting is carried out, and the vacuum degree is controlled to reach 0.05Pa. After all the raw materials are melted, the smelting power is kept constant for 20 minutes; the vacuum degree is increased to 0.005Pa. Refining at ℃ for 7 minutes, adjusting the composition to meet the requirements; then adjusting to 1610℃ and pouring into ingots; then heat treatment, first heating the ingot to 1260℃, keeping it for 4 hours, then air cooling to room temperature; then heating to 1150℃, and keeping it for 4 hours , air-cooled to room temperature; then heated to...

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Abstract

The invention discloses a method for preparing high temperature resistant nickel base alloy. The nickel base alloy consists of the following components in percentage by weight: 26.0 to 28.0 percent of Cr, 5.3 to 5.7 percent of Co, 8.2 to 8.6 percent of Mo, 2.4 to 2.8 percent of W, 0.4 to 0.6 percent of V, 3.8 to 4.2 percent of Ta, 5.6 to 6.0 percent of Al, 1.3 to 1.7 percent of Ti, 2.1 to 2.5 percent of Nb, 0.004 to 0.006 percent of B, more than or equal to 0.1 percent and less than or equal to 0.4 percent of Cu, more than 0 percent and less than or equal to 0.08 percent of C, more than 0 percent and less than or equal to 0.3 percent of Si, more than 0 percent and less than or equal to 0.5 percent of Mn, and the balance of Ni; the method for preparing the high temperature resistant nickel base alloy comprises the following steps of: mixing the components of the alloy, smelting, controlling vacuum degree to be 0.01 to 0.1Pa, and fully melting all raw materials, and then keeping smelting power constant for 15 to 25 minutes; improving the vacuum degree to be about 0.001 to 0.01Pa, refining at the temperature of between 1,650 and 1,670 DEG C for 6 to 8 minutes, and adjusting the components to ensure that the components meet the requirement; adjusting temperature to be 1,600 to 1,620 DEG C, and pouring to obtain ingots; performing heat treatment, heating the cast ingots to be 1,250 to 1,270 DEG C, preserving heat for 3 to 5hours, performing air cooling to room temperature, heating to 1,140 to 1,160 DGE C, preserving heat for 3 to 5 hours, and performing air cooling to room temperature; and heating to 1,050 to 1,070 DEG C, preserving heat for 30 to 36 hours, and performing air cooling to room temperature.

Description

technical field [0001] The invention relates to the field of alloy metals, in particular to a method for preparing a high-temperature-resistant nickel-based alloy. Background technique [0002] Superalloys refer to a class of metal materials based on iron, nickel, and cobalt that can work for a long time at high temperatures above 600°C and under certain stresses. For half a century, the temperature before the turbine of the aero-engine has increased from 730°C in the 1940s to 1677°C. The increase in service temperature puts forward more and more stringent requirements on the materials of aero-engines. Nickel-based superalloys are by far the most superior performance and the most widely used aero-engine materials. At present, the upper limit temperature of the alloy's service temperature has reached about 1200 ° C, which is close to the melting point of the alloy, but it is still the material of choice for the key components with the highest temperature and the largest str...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C30/02C22F1/00
Inventor 叶绿均
Owner 瑞安市劲力机械制造有限公司
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