Composition for anti-glaring film
An anti-glare film and composition technology, applied in the direction of coatings, polycarbonate coatings, etc., can solve the problems of easy aging deformation, reduced anti-glare effect, difficult shell refractive index, etc., to improve image clarity and contrast, Good light transmittance and simple preparation process
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[0051] The preparation method of the anti-glare film of the present invention comprises the following steps: 1) preparing anti-glare inorganic particles; 2) preparing an anti-glare film composition; 3) coating the composition on a transparent substrate; 4) curing the composition to form an anti-glare film .
[0052] Step 1) Prepare anti-glare inorganic particles with an average surface roughness of 0.01-3 μm by chemical or physical methods; Step 2) Uniformly incorporate anti-glare inorganic particles into the transparent matrix by melt mixing or solvent dissolution mixing; Step 3 ) using wet coating, rod coating, spray coating, dip coating, spin coating, etc., the coating method is not limited thereto, but various coating methods known in the art can be used; Step 4) can be divided into two parts, drying and curing, or can be completed in one step.
Embodiment 1
[0054] 1) Preparation of silica antiglare particles:
[0055] At room temperature, add 8 mL of ammonia water (25%~28%), 10 mL of H 2 O. 100mL of absolute ethanol, after mixing evenly, drop 15mL of tetraethyl orthosilicate / 100mL of absolute ethanol solution at a rate of 10mL / min, centrifuge after 4 hours of reaction, wash with water 3 times, and dry at 70°C to obtain a rough surface silica particles (such as Figure 9 );
[0056] 2) Preparation of anti-glare film composition
[0057] Dissolve 10g of PVB in 150mL of absolute ethanol, stir well, then add 0.1g of the silica particles prepared in step 1) to the transparent solution;
[0058] 3) Preparation of anti-glare film: apply the composition solution prepared in step 2) on the washed glass slide by pulling method;
[0059] 4) Place the slides obtained in step 3) in an oven at 70°C and dry overnight.
Embodiment 2
[0061] At room temperature, add 8 mL of ammonia water (25%~28%), 10 mL of H 2 0. 100 mL of absolute ethanol, after mixing evenly, drop 15 mL of tetraethyl orthosilicate / 100 mL of absolute ethanol solution at 5 mL / min, centrifuge after 4 hours of reaction, wash with water 3 times, and dry at 70° C. Silica particles (such as Figure 10 ); then by using the same method as in Example 1 to prepare a composition for an anti-glare film, and then use the composition to prepare an anti-glare film.
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