Method for preparing xylose by using squeezed waste alkali in viscose fiber production process
A technology for squeezing waste caustic soda and production process, applied in sugar production, sugar production, application, etc., can solve the problems of shortage of bamboo and other raw materials, low utilization rate of resources, etc., achieve complete hydrolysis, reduce operation steps and time short effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0057] A method for preparing xylose by pressing waste lye in the viscose fiber production process, comprising the following process steps:
[0058] A, the preparation of hemicellulose solution: the waste lye of pressing that contains alkali and hemicellulose is passed through prefiltration, precision filtration and membrane filtration successively, obtains permeate and concentrated lye, and the alkali content in the concentrated lye is 120g / L, the hemicellulose content is 40g / L;
[0059] B, the extraction of hemicellulose: with the concentrated lye obtained in step A, adjust the pH value of the supernatant to 4 with 98.5% concentrated sulfuric acid at room temperature, then add 95% industrial ethanol of 2 times the volume of the concentrated lye , let stand to precipitate, filter, wash with 95% industrial ethanol of 0.5 times the volume of concentrated lye, and dry to constant weight at a vacuum of 0.08Mpa and a drying temperature of 60°C to obtain a white hemicellulose powd...
Embodiment 2
[0075] A method for preparing xylose by pressing waste lye in the viscose fiber production process, comprising the following process steps:
[0076] A, the preparation of hemicellulose solution: the waste lye of pressing that contains alkali and hemicellulose is passed through pre-filtration, precision filtration and membrane filtration successively, obtains permeate and concentrated lye, and the alkali content in the concentrated lye is 230g / L, the hemicellulose content is 70g / L;
[0077] B, the extraction of hemicellulose: with the concentrated lye obtained in step A, adjust the pH value of the supernatant with 98.5% concentrated sulfuric acid at room temperature, then add 95% industrial ethanol of 3 times the volume of the concentrated lye , let stand to precipitate, filter, wash with 95% industrial ethanol of 1 volume of concentrated lye, and dry to constant weight at a vacuum of 0.1Mpa and a drying temperature of 80°C to obtain a white hemicellulose powder;
[0078] C, ...
Embodiment 3
[0093] A method for preparing xylose by pressing waste lye in the viscose fiber production process, comprising the following process steps:
[0094] A, the preparation of hemicellulose solution: the waste lye of pressing that contains alkali and hemicellulose is passed through pre-filtration, precision filtration and membrane filtration successively, obtains permeate and concentrated lye, and the alkali content in the concentrated lye is 175g / L, the hemicellulose content is 55g / L;
[0095]B, the extraction of hemicellulose: with the concentrated lye obtained in step A, adjust the pH value of the supernatant to 4.5 with 98.5% concentrated sulfuric acid at room temperature, then add 95% industrial ethanol of 2.5 times the volume of the concentrated lye , let stand to precipitate, filter, wash with 95% industrial ethanol of 0.75 times the volume of concentrated lye, and dry to constant weight at a vacuum of 0.09Mpa and a drying temperature of 70°C to obtain a white hemicellulose...
PUM
Property | Measurement | Unit |
---|---|---|
Conductivity | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com