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Method for controlling nitrogen content of high-permeability-grade oriented electrical steel belt

A technology of oriented electrical steel and high magnetic permeability, which is applied in the field of steelmaking, can solve the problems of difficult to meet, high cost, unstable nitrogen absorption rate, etc., and achieve the requirements of simple method, strong applicability, and secondary recrystallization Effect

Active Publication Date: 2012-08-15
SHOUGANG ZHIXIN QIAN AN ELECTROMAGNETIC MATERIALS CO LTD
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AI Technical Summary

Problems solved by technology

In order to meet the nitrogen content control requirements in the production of high-permeability grade grain-oriented electrical steel, the method of nitrogen increase control by adding nitrided alloys has been adopted at home and abroad, but the nitrogen increase control of nitrided alloys has the situation that the nitrogen absorption rate of steel liquid is unstable. , it is difficult to meet the requirement of controlling the N content of molten steel within ±5ppm accuracy
At home and abroad, the RH refining process is also used to switch between N gas and Ar gas to control liquid steel nitrogen. This method requires equipment modification, and the cost of using Ar gas is also higher than that of N gas treatment throughout the process.

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  • Method for controlling nitrogen content of high-permeability-grade oriented electrical steel belt
  • Method for controlling nitrogen content of high-permeability-grade oriented electrical steel belt

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Embodiment Construction

[0017] The technical solution of the present invention will be described in detail below in conjunction with the accompanying drawings and embodiments.

[0018] The invention provides a method for controlling the nitrogen content of a high-permeability grade-oriented electrical steel strip, which specifically includes the following steps:

[0019] (1) After the molten steel reaches the RH refining furnace, it is connected to the bottom blowing nitrogen gas, and the molten steel is blown with nitrogen, and the flow rate of the bottom blowing nitrogen gas is 18-60m 3 / h.

[0020] (2) In the initial stage of RH refining treatment, the ultimate vacuum treatment is adopted, the RH ultimate vacuum degree is ≤200Pa, the RH vacuum chamber adopts nitrogen circulation throughout, and the nitrogen circulation flow rate is 50-100m 3 / h.

[0021] (3) After 12-15 minutes of ultimate vacuum treatment, according to the initial nitrogen content of molten steel, reset the RH vacuum degree to ...

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Abstract

The invention relates to the technical field of steelmaking, in particular to a method for controlling the nitrogen content of a high-permeability-grade oriented electric steel belt. The method particularly includes following steps that molten steel is connected with bottom flushing nitrogen after reaching an RH (relative humidity) refining furnace, and nitrogen flushing treatment is performed for the molten steel; ultimate vacuum treatment is performed at the preliminary stage of RH refining treatment, RH ultimate vacuum degree is smaller than or equal to 200Pa, and nitrogen circulates in anRH vacuum chamber in the whole process; and after the ultimate vacuum treatment is performed for 12 minutes to 15 minutes, RH vacuum degree is reset according to the initial nitrogen content of the molten liquid, RH refining nitrogen adding treatment is performed, and the RH vacuum degree is reduced after a nitrogen adding target value is reached. By means of reasonably controlling nitrogen flow and the RH vacuum degree in an RH refining process, requirements on nitrogen content precision for production of the high-permeability-grade oriented electric steel belt are met. Besides, the method is simple, is high in applicability, and does not affect controlling to purity and H content of the high-permeability-grade oriented electric steel belt.

Description

technical field [0001] The invention relates to the technical field of steelmaking, in particular to a method for controlling the nitrogen content of a high-permeability grade oriented electrical steel strip. Background technique [0002] High magnetic permeability grade oriented electrical steel strip requires that the N content of molten steel should be controlled stably at ±5ppm. By stably controlling the N content and Als content of molten steel, quantitative and fine dispersed AlN will be formed in the hot rolling and normalized pickling process. As an inhibitor, AlN inhibits the growth of primary grains, forms Goss texture through secondary recrystallization during high temperature annealing, and produces oriented electrical steel strips with good magnetic properties. In order to meet the nitrogen content control requirements in the production of high-permeability grade grain-oriented electrical steel, the method of nitrogen increase control by adding nitrided alloys h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C21C7/10C21C7/072
Inventor 龚坚王国连靳伟张涛朱江波王现辉南晓东刘珍童
Owner SHOUGANG ZHIXIN QIAN AN ELECTROMAGNETIC MATERIALS CO LTD
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