Acrylic acid textile size and preparation method thereof
A technology of textile pulp and acrylic, which is applied in textiles, papermaking, fiber treatment, etc. It can solve the problems of not being able to use a large amount, poor water solubility and water dispersibility, and low strength of the size film, and achieve low hygroscopicity and yarn hairiness. , The effect of increasing yarn strength
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Embodiment 1
[0040] Raw materials: methyl acrylate (MA), butyl acrylate (BA), acrylic acid (AA), acrylamide (AM), ammonium persulfate (APS), complex emulsifier, ammonia water and deionized water, of which
[0041] 7 parts methyl acrylate
[0042] Butyl acrylate 12 parts
[0043] Acrylic 11 parts
[0044] 3 parts acrylamide
[0045] Initiator 0.8 parts
[0046] Compound emulsifier 6 parts
[0047] Ammonia 6 parts
[0048] 55 parts of deionized water;
[0049] Described composite emulsifier is the mixture of fatty alcohol polyoxyethylene ether AEO-5 and AEO-7, and the mass ratio of the two is: 2:3
[0050]Synthesis method: Add deionized water, acrylamide, acrylic acid and compound emulsifier into a three-necked flask with a volume of 1000ml, and then add 25%-35% of the mixed monomer of methyl acrylate and butyl acrylate, and then carry out Stir and raise the temperature to 88°C-93°C, add the ammonium persulfate aqueous solution and the remaining monomer mixed with methyl acrylate and ...
Embodiment 2
[0052] The difference between the present embodiment and embodiment 1 is that the weight parts consumption of each raw material is as follows:
[0053] 5 parts methyl acrylate
[0054] Butyl acrylate 15 parts
[0055] Acrylic 8 parts
[0056] Acrylamide 5 parts
[0057] Initiator 0.5 parts
[0058] Compound emulsifier 5 parts
[0059] Ammonia 5 parts
[0060] 50 parts of deionized water.
Embodiment 3
[0062] The difference between the present embodiment and embodiment 1 is that the weight parts consumption of each raw material is as follows:
[0063] 8 parts methyl acrylate
[0064] Butyl acrylate 10 parts
[0065] Acrylic 15 parts
[0066] 2 parts acrylamide
[0067] Initiator 1 part
[0068] Compound emulsifier 10 parts
[0069] Ammonia 8 parts
[0070] 60 parts of deionized water.
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