Method for preparing lanthanum cuprate (La2CuO4) powder by means of microwave-hydrothermal method
A technology of microwave hydrothermal method and lanthanum cuprate, applied in chemical instruments and methods, copper compounds, inorganic chemistry, etc., can solve the problems of easy sintering, time-consuming, poor safety performance of products, etc., to overcome uneven heating, shorten Response time, the effect of improving work efficiency
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Embodiment 1
[0019] 1) Get 50ml distilled water and add in the beaker, then add analytically pure lanthanum nitrate (La(NO) in the beaker 3 ) 3 ·6H 2 O) magnetic stirring makes concentration be the solution A of 0.6mol / L;
[0020] 2) Add analytically pure copper nitrate (Cu(NO 3 ) 3 ·3H 2 O) stirring and making copper nitrate concentration is solution B of 0.3mol / L;
[0021] 3) press citric acid (C 6 h 8 o 7 ·H 2 O) and metal cation sum are 3: 1, add analytically pure citric acid (C) in solution B in the mol ratio 6 h 8 o 7 ·H 2 O) stirring at normal temperature to obtain solution C;
[0022] 4) Add ammonia water with a mass percentage of 4% to solution C dropwise, adjust the pH to 3, and stir for 30 minutes to obtain solution D;
[0023] 5) Add solution D into the microwave hydrothermal reaction tank, and control the filling degree to 70%; after sealing the reaction tank, place it in a microwave hydrothermal instrument; control the hydrothermal temperature at 200°C, react fo...
Embodiment 2
[0027] 1) Get 45ml distilled water and add in the beaker, then add analytically pure lanthanum nitrate (La(NO) in the beaker 3 ) 3 ·6H 2 O) magnetic stirring makes concentration be the solution A of 0.5mol / L;
[0028] 2) Add analytically pure copper nitrate (Cu(NO 3 ) 3 ·3H2 O) stirring and making copper nitrate concentration is solution B of 0.5mol / L;
[0029] 3) press citric acid (C 6 h 8 o 7 ·H 2 O) and metal cation sum are 2.8: 1, and in solution B, add analytically pure citric acid (C 6 h 8 o 7 ·H 2 O) stirring at normal temperature to obtain solution C;
[0030] 4) Add ammonia water with a mass percentage of 3% to solution C dropwise, adjust the pH to 1.5, and stir for 10 minutes to obtain solution D;
[0031] 5) Add solution D into the microwave hydrothermal reaction tank, and control the filling degree to 80%; after sealing the reaction tank, place it in a microwave hydrothermal instrument; control the hydrothermal temperature at 160 ° C, react for 60 minu...
Embodiment 3
[0034] 1) Get 60ml distilled water and add in the beaker, then add analytically pure lanthanum nitrate (La(NO) in the beaker 3 ) 3 ·6H 2 O) magnetic stirring makes concentration be the solution A of 0.7mol / L;
[0035] 2) Add analytically pure copper nitrate (Cu(NO 3 ) 3 ·3H 2 O) stirring and making copper nitrate concentration is solution B of 0.4mol / L;
[0036] 3) press citric acid (C 6 h 8 o 7 ·H 2 O) and metal cation sum are 3.8: 1, the mol ratio adds analytically pure citric acid (C in solution B) 6 h 8 o 7 ·H 2 O) stirring at normal temperature to obtain solution C;
[0037] 4) Add ammonia water with a mass percentage of 5% to solution C dropwise, adjust the pH to 5, and stir for 120 minutes to obtain solution D;
[0038] 5) Add solution D into the microwave hydrothermal reaction tank, and control the filling degree to 60%; after sealing the reaction tank, place it in the microwave hydrothermal instrument; control the hydrothermal temperature at 220 ° C, rea...
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