Preparation method of high temperature heat storage material for solar photo-thermal power generation
A heat storage material and photothermal power generation technology, which is applied in heat exchange materials, chemical instruments and methods, etc., can solve the problems of limited inorganic salt content, complex process and high cost, and achieve the effect of increasing added value.
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Embodiment 1
[0015] Take polyaluminum chloride (Al 2 o 3 The content is 11.19%, the basicity is 43.20) 100mL, heated and stirred until the molten salt is precipitated, the heating temperature is 80°C, and the stirring speed is 55rpm. Increase the stirring intensity to 100 rpm, adjust the temperature to 55° C., continue stirring until a gel appears, stop stirring and cool to form a heat storage material precursor. The precursor is dried in an oven at 90°C for 3 hours, then calcined at 600°C for 3 hours, and cooled to become a heat storage material. The phase change latent heat of the material tested by SDT Q600 synchronous thermal analyzer is 35.5J g -1 , and the phase transition temperatures are 491.9°C and 538.7°C.
Embodiment 2
[0017] Take polyaluminum chloride (Al 2 o 3 The content is 11.59%, the basicity is 45.20) 100mL, heated and stirred until the molten salt is precipitated, the heating temperature is 75°C, and the stirring speed is 60rpm. Increase the stirring intensity to 105rpm, adjust the temperature to 50°C, continue stirring until gel-like, stop stirring and cool to form a heat storage material precursor. The precursor is dried in an oven at 100°C for 2 hours, then calcined at 700°C for 2 hours, and cooled to become a heat storage material. The phase change latent heat of the material tested by SDT Q600 synchronous thermal analyzer is 49.1J g -1 , and the phase transition temperatures are 492.8°C and 534.5°C.
Embodiment 3
[0019] Take polyaluminum chloride (Al 2 o 3 The content is 13.09%, the basicity is 80.00) 100mL, heated and stirred until the molten salt is precipitated, the heating temperature is 70°C, and the stirring speed is 50rpm. Increase the stirring intensity to 100rpm, adjust the temperature to 45°C, continue stirring until a gel appears, stop stirring and cool to form a heat storage material precursor. Put the precursor in an oven at 110°C for 1 hour, then bake it at 800°C for 1 hour, and cool it down to become the heat storage material. The phase change latent heat of the material tested by SDT Q600 synchronous thermal analyzer is 80.7J g -1 , the phase transition temperature is 797.3°C.
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