A kind of preparation method of humic acid coated urea
The technology of humic acid urea and coating urea is applied in the field of preparation of humic acid-coated urea, and can solve problems such as difficulty in large-scale industrial production and popularization and application, failure to improve urea fertilizer efficiency and utilization rate, and increase in production cost, etc. Achieve the effect of short production process, smooth and beautiful appearance, and reduce physical labor.
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Embodiment 1
[0024] Example 1: Take 200 parts of water into the reactor, add 40 parts of urea, stir and dissolve at about 55°C, add 80 parts of Inner Mongolia Wuchuan weathered lignite (30 mesh) containing 44% humic acid (dry basis) and 26.5% water , The temperature is raised to about 95°C for 10 minutes, 8 parts of diammonium phosphate are added, and the reaction is continued for 50 minutes with stirring. The solid-liquid separation is performed. The clear liquid contains 14.3% of water-soluble humic acid and 9.2% of N. The clear liquid is concentrated, and the concentrated liquid contains 20.4% of water-soluble humic acid and 12.6% of N. Then the concentrated liquid is dried to obtain a solid humic acid urea complex. The solid product contains 38% water-soluble humic acid and 28% N.
Embodiment 2
[0025] Example 2: Take 200 parts of water into the reactor, add 48 parts of urea, stir and dissolve at about 55°C, add 80 parts of Inner Mongolia Wuchuan weathered lignite (30 mesh) containing 69% humic acid (dry basis) and 28% water , The temperature is raised to about 95°C for 10 minutes, 8 parts of diammonium phosphate are added, the reaction is continued for 45 minutes, cooling, solid-liquid separation, the supernatant is concentrated and dried to obtain 71 parts of solid humic acid urea, containing 28 parts of humic acid, The extraction rate of humic acid is 70%, containing 47% of water-soluble humic acid and 30% of N.
Embodiment 3
[0026] Example 3: Add 91 parts of urea to the coating machine (or turntable or drum granulation equipment), and pump 25 parts of the humic acid urea complex concentrate prepared in the above example 1 into the coating machine (or Rotary table, rotary drum granulation equipment), dried at the inlet temperature of 120°C and outlet temperature of 80°C to obtain humic acid-coated urea. The product has been tested by NY 1106-2006 and GB 2441 methods. The product composition is: moisture 4.2%, Total nitrogen 44.1%, water-soluble humic acid 5.2%, pH value (1:250 times aqueous solution): 7.6.
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