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Polypropylene antistatic composite material and preparation method thereof

A composite material, polypropylene technology, used in chemical instruments and methods, fibrous fillers, inorganic pigment processing, etc., to achieve wide application prospects, stable processing performance and reliable quality assurance.

Inactive Publication Date: 2012-10-24
TAIYUAN UNIVERSITY OF SCIENCE AND TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The material can overcome the defects in the performance of various conductive fiber modified polypropylene antistatic composite materials

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] (1), aluminum borate whisker is carried out pretreatment, and its steps are:

[0018] ①Weigh 25g of aluminum borate whiskers provided by Shenyang Meixi Fine Chemical Co., Ltd. and add it to 230mL distilled water, and stir evenly; ②Weigh 18.6mL concentrated hydrochloric acid and add it to the mixed solution formed in step ①, so that the concentration of hydrochloric acid reaches 0.9mol· L -1 ; ③ 40mL tin tetrachloride is added to the mixed solution formed in step ②, and stirred evenly; ④ 95g urea is added to the mixed solution formed in step ③; React in a constant temperature water bath at this temperature for 1.5 hours under normal pressure; ⑥ filter the mixed solution obtained in step ⑤ to obtain aluminum borate whiskers loaded with tin oxide precursor precipitation products; Wash the aluminum borate whiskers obtained in step ⑥ to remove unreacted reactants; ⑧ place the aluminum borate whiskers obtained in step ⑦ in a drying oven at 85°C for 8 hours; ⑨ dry the dried a...

Embodiment 2

[0022] (1), aluminum borate whisker is carried out pretreatment, and its steps are:

[0023] ①Weigh 35g of aluminum borate whiskers provided by Qinghai Haixing Science and Technology Development Co., Ltd. and add it to 250mL of distilled water, and stir evenly; ②Weigh 17.8mL of concentrated hydrochloric acid and add it to the mixed solution formed in step ① to make the concentration of hydrochloric acid reach 0.8mol · L -1 ; ③ 50mL tin tetrachloride is added to the mixed solution formed in step ②, and stirred evenly; ④ 100g urea is added to the mixed solution formed in step ③; React in a constant temperature water bath at this temperature for 2 hours under normal pressure; ⑥ filter the mixed solution obtained in step ⑤ to obtain aluminum borate whiskers loaded with tin oxide precursor precipitation products; Wash the aluminum borate whiskers obtained in step ⑥ to remove unreacted reactants; ⑧ place the aluminum borate whiskers obtained in step ⑦ in a drying oven at 90°C for 7...

Embodiment 3

[0027] (1), aluminum borate whisker is carried out pretreatment, and its steps are:

[0028] ①Weigh 28g of aluminum borate whiskers provided by Shanghai Fengzhu Whisker Co., Ltd. and add them to 250mL of distilled water, and stir evenly; ②Weigh 22.7mL of concentrated hydrochloric acid into the mixed solution formed in step ①, so that the concentration of hydrochloric acid reaches 1.0mol· L -1 ; ③ 40mL tin tetrachloride is added to the mixed solution formed in step ②, and stirred evenly; ④ 95g urea is added to the mixed solution formed in step ③; React in a constant temperature water bath at this temperature for 3 hours under normal pressure; ⑥ filter the mixed solution obtained in step ⑤ to obtain aluminum borate whiskers loaded with tin oxide precursor precipitation products; ⑦ use distilled water first, and then dehydrate Wash the aluminum borate whiskers obtained in step ⑥ to remove unreacted reactants; ⑧ place the aluminum borate whiskers obtained in step ⑦ in a drying ov...

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Abstract

The invention relates to a polypropylene antistatic composite material and a preparation method thereof, belonging to the technical field of polypropylene composite materials. The invention is characterized in that the polypropylene antistatic composite material contains conductive aluminum borate whiskers, and is AlB[w] / PP for short. The preparation method comprises the following steps: proportionally adding aluminum borate whiskers into distilled water, adding concentrated hydrochloric acid so that the acid concentration reaches 0.6-1.2 mol.L<-1>, proportionally adding tin tetrachloride andurea, heating the mixed liquor to 90-110 DEG C, reacting for 1-3 hours, filtering, washing to remove unreacted substances, drying the filter cake, and calcining to obtain conductive aluminum borate whiskers (AlB[w] for short); and proportionally mixing the AlB[w] and polypropylene, mixing, crushing, putting the mixture in a die, putting the die in a muffle furnace at 180-200 DEG C, keeping the temperature for 30-60 minutes, carrying out die forming in a flat vulcanizing machine, and depressurizing and stripping when the temperature of the die drops to below 60 DEG C, thereby obtaining the AlB[w] / PP.

Description

technical field [0001] The invention belongs to the technical field of polypropylene composite materials, and in particular relates to a polypropylene antistatic composite material and a preparation method thereof. Background technique [0002] During production, processing and use, polymers are often charged with static electricity when they come into contact with other materials and devices. For example, during the spinning process of polyacrylonitrile fibers, the static electricity generated by friction can reach more than 1500 volts. The accumulation of fiber stretching static electricity can even reach tens of thousands of volts. Generally speaking, static electricity is an unfavorable factor in the process of polymer processing and use, because static electricity hinders normal processing technology, static electricity damages product quality, and may even endanger personal and equipment safety. Due to the rich source of raw materials and the excellent characteristic...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L23/12C08K9/02C08K7/08C09C1/40C09C3/06B29C43/58C09K3/16
Inventor 金亚旭田玉明于晓璞杨雯闫时建
Owner TAIYUAN UNIVERSITY OF SCIENCE AND TECHNOLOGY
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