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Preparation method for black marking glaze for borosilicate glass insulator

A borosilicate glass, insulator technology, applied in insulators, electrical components, circuits, etc., can solve the problems of failing to achieve marking, falling off of marked numbers and letters, reducing insulators, etc., achieving convenient operation, strong three-dimensional effect, and deep glaze color. black effect

Inactive Publication Date: 2012-10-03
LIAONING SILICATE RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the high sintering temperature in the sealing process, ordinary organic colorants decompose at high temperatures and fail to achieve the purpose of marking; while ordinary inorganic colorants will reduce the surface resistance of the insulator, and the post-processing of the sealed socket During the process, after chemical polishing and gold-plated pins, it is easy to cause marking numbers and letters to fall off, which cannot meet the marking requirements

Method used

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Experimental program
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Embodiment Construction

[0011] The present invention is achieved through the following process steps:

[0012] 1. Using various chemically pure oxides as basic raw materials, its main formula is designed as (by weight %) SiO 2 40%-60%, B 2 o 3 10%-20%, ZnO 2%-7%, Na 2 O 3%-5%, Fe 2 o 3 5%-8%, Mn 3 o 4 3%-8%, Al 2 o 3 1%-5%. Then the batch material was melted at 1500° C. for 3 hours and then water-quenched to obtain the basic glass.

[0013] 2. The basic glass is crushed by a jaw crusher, cleaned, and then ground by a ball mill until it is finely ground to 160 mesh, and dried for later use.

[0014] 3. Mix the dried glass frit with organic solvent (varnish), the mixing ratio is powder:organic solvent=45~85:100, and a small amount of diluent (for varnish) should be added during the mixing process thinner) to make a black marker glaze.

[0015] 4. Put the prepared marking glaze on the screen printing table, and perform screen printing on the fired glass insulator.

[0016] 5. After the...

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PUM

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Abstract

The invention provides a preparation method for black marking glaze for a borosilicate glass insulator. The preparation method comprises the following steps of: adjusting a proper burdening point by taking various chemical pure oxides as basic raw materials, sintering at the high temperature, and water-quenching to obtain basic glass; smashing and grinding, and mixing the smashed basic glass and an organic solvent to obtain the black marking glaze; and finally printing the prepared marking glaze through a silk screen. The preparation method for the black marking glaze for the borosilicate glass insulator has the advantages that: 1, in the preparation method, the marking glaze is prepared by mixing the organic solvent and an inorganic glass material; the marking glaze prepared by the method is encapsulated by an atmosphere furnace at the high temperature and subjected to post chemical polishing, so letters or numbers marked by the marking glaze are hard to fall off and clear, and shortlines and decoloration phenomena are avoided; and the appearance quality of a sealed socket meets the requirements; 2, the marking glaze which is prepared by the method and subjected to the whole test of the sealed socket has no influence on the electric insulation performance; and 3, the marking glaze prepared by the method is directly printed on a glass blank cake, and the glaze is deep black in color, strong in stereoscopic sensation, clear to see words, convenient to operate and simple in process.

Description

technical field [0001] The invention relates to a preparation method, in particular to a preparation method of a black marking glaze for borosilicate glass insulators, and belongs to the technical field of new material manufacture and application. Background technique [0002] The sealed socket of the stainless steel shell is the key component of the connection of the electrical circuit. It has high requirements on the performance of the product. The glass insulator and the metal are hermetically sealed, which is far stronger than the conventional seal. The hermetic seal can withstand higher temperatures and Pressure, and can always provide an effective barrier against humid air pollutants or other pollutants. This high-end electrical connector is mostly used in many critical occasions such as aircraft, petrochemical, and electronic industries. [0003] Borosilicate insulating glass has the advantages of good insulation, strong voltage resistance, good chemical stability aga...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01B19/04C03C8/00C03C17/00
Inventor 张明韩绍娟许壮志薛健亢永珍张莹莹
Owner LIAONING SILICATE RES INST
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