Expanded vitrified micro-bead fireproof thermal-insulation board and preparation method thereof
A technology of expanding vitrified microbeads and fireproof insulation boards, which is applied in the field of building materials, can solve the problems of general insulation effect, complicated manufacturing process, and small thermal conductivity, and achieves reliable strength, safety and stability, simple preparation process, and surface glass. The effect of closing
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preparation example Construction
[0031] The preparation method of expanded vitrified microbead fireproof insulation board,
[0032] ①Material preparation: Take 50-200 parts of binder, 0-10 parts of curing agent hexamethylenetetramine, 0-200 parts of solvent and stir evenly, and mix them with 100 parts of expanded vitrified microbeads;
[0033] ②Preforming treatment: Put the material treated in ① into a flat mold and compact it to smooth it out. The compression ratio is 1:1:1~1:1.3. Put the flat mold and the material in the heating device for heating and forming The heating temperature is 150°C-300°C, and the heating time is 3-30 minutes;
[0034] ③ Sintering molding: demoulding the preformed sheet, placing the sheet in the heating device, and then injecting nitrogen gas into the heating device at a rate of 10-100ml / min, sintering and molding, the sintering temperature is 200 ° C ~ 900 ° C, The sintering time is 20 minutes to 5 hours.
[0035] When the binding agent that adopts is phenolic resin, its prepara...
Embodiment 1
[0045] Take 50 parts of phenolic resin (PFn-5420), 2.5 parts of hexamethylenetetramine, add 110 parts of ethanol to dilute, take 100 parts of expanded vitrified microbeads, mix it with the above resin solution, and compress according to 1:1.1 After injecting into the mold of the required specifications, compact and smooth it, put it in an oven at 150°C for 30 minutes for pre-forming treatment, after demoulding, put the formed plate in the oven, raise the temperature to 200°C and put that at the same time Nitrogen gas is passed into the oven at a rate of 10 ml / min, and sintered for 2 hours under the condition of nitrogen atmosphere to obtain the expanded vitrified bead fireproof insulation board of the present invention. Its bulk density is 108kg / m 3 , thermal conductivity 0.045m·K, fire resistance class A.
Embodiment 2
[0047] Take 60 parts of phenolic resin (PFn-5420), 3.0 parts of hexamethylenetetramine, add 100 parts of ethanol to dilute, take 100 parts of expanded vitrified microbeads, mix it with the above resin solution, and compress according to the ratio of 1:1.2 After injecting into the mold of the required specifications, compact and smooth, put it in an oven at 180°C for 30 minutes for pre-forming treatment, after demoulding, place the formed plate in a muffle furnace, raise the temperature to 450°C and At the same time, feed nitrogen gas into the muffle furnace at a rate of 20 ml / min, and sinter for 2 hours under the condition of nitrogen atmosphere to obtain the expanded vitrified microbead fireproof insulation board of the present invention. Its bulk density is 128kg / m 3 , thermal conductivity 0.043m·K, fire resistance class A.
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