Photonic crystal micro-nano structure direct-writing method based on metal nanoparticles
A metal nanoparticle and photonic crystal technology, applied in the directions of light guides, optics, optical components, etc., can solve the problems that limit the wide application of metal photonic crystals and the development of practical technologies, the complex preparation process and the expensive preparation equipment, etc., to improve the adhesion. And the effect of firmness, good repeatability and high preparation efficiency
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Embodiment 1
[0017] Example 1: Preparation of a one-dimensional gold nanowire photonic crystal structure.
[0018] 1) dissolving the chemically synthesized gold nanoparticles with an average diameter of 5nm in organic solvents such as toluene or xylene to make a gold nanoparticle colloid solution with a concentration of 100 mg / ml;
[0019] 2) Spin-coat the colloidal solution of gold nanoparticles on the glass substrate. The spin coating speed is 2000rpm, and the corresponding film thickness is about 200nm;
[0020] 3) Place the gold thin film sample prepared above in the interference light path, such as figure 1 As shown, the angle θ=7.8° between the two beams. Using manual triggering to make the laser emit a laser pulse with an energy of 10mJ, a pulse width of 6ns, and a wavelength of 266nm, a periodic grating structure can be etched on the gold nanoparticle film. composed of gold nanoparticles.
[0021] 4) Place the above-mentioned grating structure on a heating plate and heat it at ...
Embodiment 2
[0024] On the basis of the embodiment, the sample is rotated 90° around its normal, and then subjected to the second exposure and ablation, and then undergoes step 4) heat treatment to realize the preparation of the two-dimensional metal nano-grating structure.
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