Low-temperature co-fired ceramic medium material and preparation method thereof
A low-temperature co-fired ceramic and dielectric material technology is applied in the field of ceramic dielectric materials and their preparation, and can solve the problems of high loss, low dielectric constant, and narrow range of adjustable sintering shrinkage.
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[0018] Example Large Group 1
[0019] Raw material BaTiO 3 、 Bi 2 o 3 、Nd 2 o 3 and TiO 2 According to the formula Ba 6-3x (Nd 0.4 Bi 0.6 ) 8+2x Ti 18 o 54 , where x=0.8, batching, ball milling on a ball mill with a rotating speed of 400r / min for 6 hours, drying at 100°C in a 3.3kw ordinary oven, passing through 250 holes / cm 2 Sieve the sample, raise the temperature to 980°C at 5°C / min, and keep it at 980°C for 3 hours to obtain frit A. According to the proportions stated in the table below, the molten water is cooled, ground, and sieved to obtain glass powder B and glass powder C
[0020] Element
Li 2 CO 3 (g)
SiO 2 (g)
h 3 BO 3 (g)
LiF(g)
BaF 2 (g)
total
Glass Powder B
40
10
50
0
0
100
Glass Powder C
0
0
0
20
80
100
[0021] Carry out secondary batching, ball mill on a ball mill at a speed of 400r / min for 8 hours, dry at 120°C, pass throu...
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