Double-coated pressure sensitive adhesive sheet for fixing flexible printed circuit board
A flexible printing and adhesive sheet technology, applied in the directions of laminated printed circuit boards, printed circuits, printed circuit manufacturing, etc. The effects of excellent followability, improved quality, and good workability
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Embodiment 1
[0101]93 parts by weight of butyl acrylate, 7 parts by weight of acrylic acid and 0.05 parts by weight of 4-hydroxybutyl acrylate are solvent-polymerized with ethyl acetate and 0.1 part by weight of azobisisobutyronitrile as an initiator by a conventional method, A solution (solid content concentration: 25% by weight) of an acrylic polymer (referred to as "acrylic polymer 1") having a weight average molecular weight of 1,500,000 was obtained. In this solution, with respect to 100 parts by weight of the acrylic polymer, 0.4 parts by weight (in terms of solid content) of an isocyanate-based crosslinking agent (manufactured by Nippon Polyurethane Industry Co., Ltd., trade name "Coroneto L"; trimethylol Toluene diisocyanate adduct of propane, solid content concentration 75% by weight) to obtain a binder solution (acrylic binder solution).
[0102] The adhesive solution obtained above was applied to both surfaces of a polyethylene terephthalate film (manufactured by Toray Co., Ltd....
Embodiment 2
[0108] As shown in Table 1, the compounding amount of the isocyanate crosslinking agent in the adhesive solution was changed, and a multifunctional epoxy crosslinking agent (manufactured by Mitsubishi Gas Co., Ltd., trade name "Tetrad C") was also used as the crosslinking agent. agent, except that, it was carried out in the same manner as in Example 1 to obtain a double-sided pressure-sensitive adhesive sheet.
[0109] In addition, the "compounding amount (parts by weight)" of the isocyanate-based crosslinking agent (Coronet L) in Table 1 represents "the compounding amount ( parts by weight)". The "compounding amount (parts by weight)" of the epoxy-based crosslinking agent (Tetrad C) means "the compounding amount (parts by weight) of Tetrad C itself (product itself) with respect to 100 parts by weight of the acrylic polymer."
Embodiment 3、4
[0110] Embodiment 3, 4, comparative example 3
[0111] As shown in Table 1, except that the thickness of the polyethylene terephthalate film used as the plastic film substrate and the thickness of the adhesive layer were changed, it was carried out in exactly the same manner as in Example 2, and a double Adhesive sheet.
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