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Stable single-component epoxy surface mount adhesive in room temperature storage and preparation method thereof

An epoxy patch, one-component technology, applied in the direction of epoxy resin adhesive, adhesive, adhesive type, etc., can solve problems such as failure, shortened service life of patch adhesive, increase of viscosity of patch adhesive, etc., to achieve Good printability and consistency, high wet strength effect

Inactive Publication Date: 2010-06-30
TONSAN ADHESIVES INC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although latent curing agents on the market that can achieve rapid curing at medium temperatures have certain latent properties at low temperatures, they will still release organic amines at room temperature, which will increase the viscosity of the patch adhesive and affect the use
Especially when combined with low-viscosity resins such as diluents, the release rate of organic amines is accelerated, resulting in unsatisfactory storage stability of patch adhesives at room temperature. Higher requirements are put forward for storage and storage, which affects the use of customers, resulting in shortened service life or failure of patch adhesives, resulting in economic waste

Method used

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  • Stable single-component epoxy surface mount adhesive in room temperature storage and preparation method thereof

Examples

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Effect test

Embodiment 1

[0027] Epoxy 128 41 parts

[0028] Resorcinol epoxy resin 10 parts

[0029] Polymerized amine epoxy resin curing agent EH4070s 26 parts

[0030] Diethylenetriamine 1 part

[0031] Dithiosalicylic acid 1.0 parts

[0032] Organic bentonite 5 parts

[0033] Magnesium oxide 15 parts

[0034] Big red powder 1.0 parts

[0035] Preparation method: Accurately weigh various raw materials according to the proportion of the above formula, now add epoxy resin, reactive diluent, filler, pigment, and stabilizer into the reaction kettle in sequence, stir evenly, then add latent curing agent, and wait until uniformly stirred , add thixotropic agent, disperse evenly, and carry out vacuum defoaming treatment.

Embodiment 2

[0037] Epoxy 128 31 parts

[0038] Epoxy resin E44 7 parts

[0039] Glycerin glycidyl ether 14 parts

[0040] Imidazole curing agent PN40 18 parts

[0041] 3 parts of imidazole curing agent PN-H

[0042] Caffeic acid 1.0 parts

[0043] Fumed silica 7 parts

[0044] Calcium carbonate 18 parts

[0045] Big red powder 1.0 parts

[0046] Preparation method: Accurately weigh various raw materials according to the proportion of the above formula, now add epoxy resin, reactive diluent, filler, pigment, and stabilizer into the reaction kettle in sequence, stir evenly, then add latent curing agent, and wait until uniformly stirred , add thixotropic agent, disperse evenly, and carry out vacuum defoaming treatment. The embodiment listed in table 1 and its curing characteristics and storage performance test results show that: the patch adhesive of the present invention has fast curing speed, high bonding strength, good room temperature stability, and long storage time, which brings...

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PUM

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Abstract

The invention discloses a stable single-component epoxy surface mount adhesive in room temperature storage and a preparation method thereof. The surface mount adhesive comprises the following components according to parts by weight: 30-45 parts of epoxy resin, 10-25 parts of epoxy diluent, 20-35 parts of latent curing agent, 0.5-2.0 parts of stabilizer, 5-15 parts of thixotropic agent, 15-30 parts of filler and 0.1-1.0 part of pigment. The preparation method comprises the following steps: (a) adding the epoxy resin, reactive diluent, the filler, the pigment and the stabilizer into a reactor for uniform mixing sequentially; (b) adding the latent curing agent into the above mixture for uniform mixing; and (c) adding the thixotropic agent for uniform dispersing and vacuum defoaming treatment.

Description

technical field [0001] The invention relates to an adhesive for surface mounting in the electronic industry, in particular to a one-component epoxy patch adhesive with room temperature storage stability and a preparation method thereof. Background technique [0002] With the development of the electronics industry, electronic appliances are developing toward miniaturization, light weight, multi-function, and high performance, and the application of surface mount technology SMT is becoming more and more common. Surface mount technology SMT, its process involves a variety of adhesive materials, such as patch glue for fixing components, sealant for positioning coils and some components, plug-in glue for temporarily bonding surface assembly components, etc. Among these adhesives, the most important thing for the SMT process is the patch adhesive, which mainly uses printing or pin dot patterns, cured by reflow soldering, and sticks the chip electronic components to a specific pos...

Claims

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Application Information

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IPC IPC(8): C09J163/00
Inventor 李建华
Owner TONSAN ADHESIVES INC
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