Method for inspecting quality of indigowoad leaf Chinese medicament
A quality inspection method and technology of Daqingye, applied in the field of natural medicinal chemistry, can solve the problem of insufficient overall control of the quality of Daqingye
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Embodiment 1
[0019] (1) Preparation of test sample solution
[0020] Using Folium Folium as raw material, weigh 2g of Folium Folium herbal decoction pieces, add 40mL of water to decoct twice, each time for 1h, filter, combine the filtrate, add ethanol 3 times the volume of the filtrate, stir well, let stand for 24h, Filtrate, concentrate under reduced pressure and dry to obtain Folium Folium water extract, add 25mL water to dissolve the obtained Folium Folium water extract, add 25mL ethyl acetate to extract 3 times respectively, combine the ethyl acetate extracts, depressurize Concentrated and dried, the residue was dissolved with 50% (V / V) methanol and fixed to 10mL and shaken up, which was the test solution 1; the extracted part was extracted 3 times by adding 25mL water-saturated n-butanol, and combined with water-saturated The n-butanol extract was concentrated under reduced pressure and dried, and the residue was dissolved in 60% (V / V) ethanol and settled to 25mL, which was the test s...
Embodiment 2
[0030] (1) Preparation of test sample solution
[0031] Using Folium Folium as raw material, weigh 4g of Folium Folium herbal decoction pieces, add 80mL of water to decoct twice, each time for 1h, filter, combine the filtrate, add ethanol 3 times the volume of the filtrate, stir well, let stand for 24h, Filtrate, concentrate under reduced pressure and dry to obtain Folium Folium water extract, add 50mL water to dissolve the obtained Folium Folium water extract, add 50mL ethyl acetate to extract 3 times respectively, combine the ethyl acetate extracts, depressurize Concentrated and dried, the residue was dissolved with 50% (V / V) methanol and fixed to 10mL and shaken up, which was the test solution 1; the extracted part was extracted 3 times by adding 50mL water-saturated n-butanol, and combined with water-saturated The n-butanol extract was concentrated under reduced pressure and dried, and the residue was dissolved in 60% (V / V) ethanol and settled to 25mL, which was the test s...
Embodiment 3
[0041] (1) Preparation of test sample solution
[0042] Using Folium Folium as raw material, weigh 6g of Folium Folium herbal decoction pieces, add 120mL of water to decoct twice, each time for 1h, filter, combine the filtrate, add ethanol 3 times the volume of the filtrate, stir well, let stand for 24h, Filtrate, concentrate under reduced pressure and dry to obtain Folium Folium water extract, add 50mL water to dissolve the obtained Folium Folium water extract, add 50mL ethyl acetate to extract 3 times respectively, combine the ethyl acetate extracts, depressurize Concentrated and dried, the residue was dissolved with 50% (V / V) methanol and fixed to 10mL and shaken up, which was the test solution 1; the extracted part was extracted 3 times by adding 50mL water-saturated n-butanol, and combined with water-saturated The n-butanol extract was concentrated under reduced pressure and dried, and the residue was dissolved in 60% (V / V) ethanol and settled to 25mL, which was the test ...
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