Preparation method for NbTi/Cu multi-core composite superconducting wire with rectangular section
A rectangular cross-section, superconducting wire rod technology, applied in the usage of superconductor elements, cable/conductor manufacturing, superconducting devices, etc., can solve the problems of difficult processing, uneven force, etc. Uniform and simple process steps
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[0037] Such as figure 1 As shown, the method for preparing the rectangular cross-section NbTi / Cu multi-core composite superconducting wire of the present invention includes the following steps:
[0038] Step 1. One-time extrusion assembly, the extrusion assembly process is as follows:
[0039] 101. The first assembly: Assemble the NbTi rod, the pure Nb liner tube and the oxygen-free copper outer sheath into a NbTi / Cu composite sheath. The NbTi / Cu composite sheath consists of a NbTi rod and a coaxial sheath in the NbTi rod. The pure Nb lining pipe on the upper side and the oxygen-free copper outer sleeve coaxially sleeved on the pure Nb inner lining pipe; the oxygen-free copper outer sleeve includes an oxygen-free copper outer tube and the oxygen-free copper outer tube One upper and lower end cover one;
[0040] 102. The first vacuum sealing welding: the upper and lower end caps described in step 101 are welded to the upper and lower ends of the oxygen-free copper outer tube by vacu...
Embodiment 1
[0055] In this embodiment, when preparing a rectangular cross-section NbTi / Cu multi-core composite superconducting wire, the main steps are as follows:
[0056] Step 1. One-time extrusion assembly, the extrusion assembly process is as follows:
[0057] 101. First assembly: First, assemble the processed Φ76mmNbTi rod, Φ100×210mm oxygen-free copper outer jacket 1 and pure Nb liner pipe into a NbTi / Cu composite jacket; and before assembly, the NbTi rod and pure Nb The inner lining pipe and the oxygen-free copper outer jacket are respectively pickled, dehydrated and dried; and when pickling is carried out, a mixed acid composed of nitric acid and water is used for the oxygen-free copper outer jacket-pickling; nitric acid and water are used The mixed acid composed of hydrofluoric acid and NbTi rods and pure Nb lined pipes are pickled, and then dehydrated with alcohol.
[0058] 102. The first vacuum sealing welding: the upper and lower end caps described in step 101 are welded to the uppe...
Embodiment 2
[0075] In this embodiment, the difference from embodiment 1 is: in the first assembly in step 101, the processed Φ76mmNbTi rod, Φ100×210mm oxygen-free copper outer sleeve 1 and pure Nb lined tube are assembled into NbTi / Cu Composite sheath; in step 207, the 7914-core NbTi / Cu obtained by the second main drawing and aging heat treatment is performed by drawing equipment and using two rectangular shaped molds with dimensions of 2.9×1.1mm and 2.7×1.0mm The composite filament is drawn in two molds and the critical current density is 2.05×10 6 A / cm 2 (4.2K, 5T) rectangular cross-section NbTi / Cu multi-core composite superconducting wire finished product. In this embodiment, the rest of the process steps, process parameters, and preparation process are the same as in Example 1.
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