Preparation method of microenvironment conditioned paper of museum
A micro-environment and humidity-adjusting paper technology, which is applied in special paper, paper, papermaking, etc., can solve the problems of wood, ancient ink cracking, embrittlement, leaving stains, and intensified deformation, achieving high moisture content and easy production , the effect of low phase transition temperature
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Embodiment 1
[0014] A preparation method of museum micro-environment humidity-regulating paper, characterized in that the following steps are adopted:
[0015] A) Add the sepiolite, artificial zeolite, gelatin, and urea that have been roasted at 250°C and activated for 2.5 hours successively into deionized water, and stir for 4 hours at a temperature of 50°C; the amount of artificial zeolite added is equal to that of sepiolite , the addition of gelatin is also equivalent to sepiolite, the addition of urea is 0.5 times of sepiolite weight, and the consumption of deionized water is 2 times of sepiolite weight;
[0016] B) successively adding acrylic acid with a concentration of 10% by weight, polyethylene glycol with a concentration of 10% by weight, ammonium persulfate and deionized water with a concentration of 1% by weight to the reactant of step A) , at a temperature of 50° C., stirring and reacting for 3 h; the addition of acrylic acid with a concentration of 10% by weight is equal to t...
Embodiment 2
[0020] A preparation method of museum micro-environment humidity-regulating paper, characterized in that the following steps are adopted:
[0021] A) Add the sepiolite, artificial zeolite, gelatin, and urea that have been roasted at 300°C and activated for 3.5 hours successively into deionized water, and stir for 6 hours at a temperature of 60°C; the amount of artificial zeolite added is equal to that of sepiolite , the addition of gelatin is also equivalent to sepiolite, the addition of urea is 0.5 times of sepiolite weight, and the consumption of deionized water is 5 times of sepiolite weight;
[0022] B) successively adding acrylic acid with a concentration of 20% by weight, polyethylene glycol with a concentration of 20% by weight, ammonium persulfate and deionized water with a concentration of 2% by weight to the reactant of step A) , at a temperature of 60° C., stirring for 5 h; the addition of acrylic acid with a concentration of 20% by weight is equal to the amount of ...
Embodiment 3
[0026] A preparation method of museum micro-environment humidity-regulating paper, characterized in that the following steps are adopted:
[0027] A) Add the sepiolite, artificial zeolite, gelatin and urea that have been roasted at 280°C and activated for 3 hours successively into deionized water, and stir for 5 hours at a temperature of 55°C; the amount of artificial zeolite added is equal to that of sepiolite, The addition of gelatin is also equal to the amount of sepiolite, the addition of urea is 0.5 times of the weight of sepiolite, and the consumption of deionized water is 4 times of the weight of sepiolite;
[0028] B) successively adding acrylic acid with a concentration of 15% by weight, polyethylene glycol with a concentration of 15% by weight, ammonium persulfate and deionized water with a concentration of 2% by weight to the reactant of step A) , at a temperature of 55° C., stirring and reacting for 4 h; the addition of acrylic acid with a concentration of 15% by w...
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