Cerium manganese co-doped yttrium (lutetium) aluminate ultra fast scintillation crystal and preparation method thereof
A scintillation crystal, yttrium aluminate technology, applied in crystal growth, chemical instruments and methods, single crystal growth and other directions, can solve the problems of long scintillation time, high light yield, slow component ratio and so on
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Embodiment 1
[0028] Embodiment 1: prepare Ce 0.001 mn 0.005 Y 0.999 Al 0.995 o 3 scintillation crystal
[0029] According to the above-mentioned process step (1) take Ce 2 o 3 , MnO 2 , Y 2 o 3 , and Al 2 o 3 , where MnO 2 The purity is 99.995%, and the rest are 99.999%; according to the above-mentioned process step (2), the above-mentioned components weighed are fully mixed into a uniform powder; according to the above-mentioned process step (3), the uniformly mixed raw materials are Under pressure, press the mixed powder into a cylindrical cake (the diameter of the cake is slightly smaller than the diameter of the crucible container), and sinter at a temperature of 1200 ° C for 10 hours; according to the above process step (4), pack the fired Enter in the Ir gold crucible in the hearth, adopt medium-frequency induction to heat the raw material in the Ir crucible to make it melt completely; Adopt the YAlO of b axis according to process step (5) 3 (YAP) crystal seeds were grow...
Embodiment 2
[0030] Embodiment 2: preparation Ce 0.01 mn 0.01 Y 0.99 Al 0.99 o 3 scintillation crystal
[0031] According to the above-mentioned process step (1), take Ce at a ratio of 0.02:0.02:0.99:0.99 with a molar ratio 2 o 3 , MnO 2 , Y 2 o 3 and Al 2 o 3 , where MnO 2 The purity is 99.995%, and the rest are 99.999%; according to the above-mentioned process step (2), the above-mentioned components weighed are fully mixed into a uniform powder; according to the above-mentioned process step (3), the uniformly mixed raw materials are Under pressure, press the mixed powder into a cylindrical cake (the diameter of the cake is slightly smaller than the diameter of the crucible container), and sinter at a temperature of 1200 ° C for 10 hours; according to the above process step (4), pack the fired Enter in the Ir gold crucible in the hearth, adopt medium-frequency induction to heat the raw material in the Ir crucible to make it melt completely; Adopt the YAlO of b axis according to...
Embodiment 3
[0032] Embodiment 3: preparation Ce 0.0001 mn 0.0001 Y 0.9999 Al 0.9999 o 3 scintillation crystal
[0033] According to the above-mentioned process step (1) take Ce 2 o 3 , MnO 2 , Y 2 o 3 and Al 2 o 3 , where MnO 2 The purity is 99.995%, and the rest are 99.999%; according to the above-mentioned process step (2), the above-mentioned components weighed are fully mixed into a uniform powder; according to the above-mentioned process step (3), the uniformly mixed raw materials are Under pressure, press the mixed powder into a cylindrical cake (the diameter of the cake is slightly smaller than the diameter of the crucible container), and sinter at a temperature of 1200 ° C for 10 hours; according to the above process step (4), pack the fired Enter in the Ir gold crucible in the hearth, adopt medium-frequency induction to heat the raw material in the Ir crucible to make it melt completely; Adopt the YAlO of b axis according to process step (5) 3 (YAP) crystal seeds wer...
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