Wet-type high cracking resistance, high wear resistance and high peel strength polyurethane resin and preparation thereof
A technology of polyurethane resin and high wear resistance, which is applied in the field of its preparation, can solve the problems of not being able to achieve high bending resistance, high wear resistance and high peeling at the same time, and achieve improved wear resistance, improved durability, good flexibility and heat resistance The effect of stability
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Embodiment approach 1
[0026] Raw material name Weight (unit: Kg)
[0027] PET-A 300
[0028] PET-B 600
[0029] Ethylene glycol 126
[0030] 4,4-Diphenylmethane diisocyanate 592
[0031] Antioxidant I-1010 2.0
[0032] Catalyst (phosphoric acid or organic bismuth catalyst MB20) 0.2
[0033] Accelerator 60
[0034] Retarder 40
[0035] Leveling agent 10
[0036] N,N-Dimethylformamide 3680
[0037] PET-A is a polyester polyol with a molecular weight of 4000. The raw materials and formula used are 4000Kg of adipic acid, 1300Kg of ethylene glycol, 900Kg of 1,4-butanediol, and 0.5Kg of catalyst TPT. (The catalyst TPT here is used for the synthesis of polyester polyol PET, while the previous organic bismuth catalyst MB20 is used for the synthesis of polyurethane resin.)
[0038] PET-B is a polyester polyol with a molecular weight of 2300. The raw materials and formula used are 3000Kg adipic acid, 190Kg ethylene glycol, 1860Kg 1,4-butanediol, and 0.4Kg catalyst TPT.
[0039] The wet type high to...
Embodiment approach 2
[0046] Raw material name Weight (unit: Kg)
[0047] PET-A 350
[0048] PET-B 550
[0049] Ethylene glycol 110
[0050] 1,4-butanediol 25
[0051] 4,4-Diphenylmethane diisocyanate 595
[0052] Antioxidant I-1010 2.0
[0053]Catalyst 0.2
[0054] Accelerator 70
[0055] Retarder 30
[0056] Leveling agent 10
[0057] N,N-Dimethylformamide 3700
[0058] PET-A is a polyester polyol with a molecular weight of 4000. The raw materials and formula used are 4000Kg of adipic acid, 1300Kg of ethylene glycol, 900Kg of 1,4-butanediol, and 0.5Kg of catalyst TPT.
[0059] PET-B is a polyester polyol with a molecular weight of 2300. The raw materials and formula used are 3000Kg adipic acid, 190Kg ethylene glycol, 1860Kg 1,4-butanediol, and 0.4Kg catalyst TPT.
[0060] The wet type high tortuous resistance, high wear resistance and high peeling polyurethane resin of the present invention is specifically prepared according to the following steps:
[0061] 1. Put polyester polyol comp...
effect approach 3
[0067] In order to verify that the wet high tortuosity, high wear resistance, and high peeling polyurethane resin described in the present invention can simultaneously achieve three performance indicators such as high tortuosity, high wear resistance, and high peeling, the resin prepared by the above embodiment is The following formula is used to make synthetic leather, and the specific leather-making formula is as follows:
[0068] Resin 100
[0069] DMF 55
[0070] B-90 1.0
[0071] S-91 2.5
[0072] Lignin 4.0
[0073] CaCO3 2.0
[0074] Appropriate amount of color paste
[0075] After testing, the wet-type polyurethane synthetic leather made with the above-mentioned formula can simultaneously have high peel strength and good bending resistance, and has high abrasion resistance.
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