Preparation of fluorescer for visualizing latent fingermark on viscous surface of adhesive tape
A fluorescent agent and sticky surface technology, which is applied in the field of fluorescent agent preparation, can solve the problem of lack of display effect of nano-type and non-nano-type display reagents, clarity of lines and details, poor selective combination with fingerprint residues, etc. problems, to achieve the effect of being suitable for mass production, improving sensitivity and accuracy, and being easy to popularize
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Embodiment 1
[0022] (1) Add 1mL of distilled water and 0.15g of sodium sulfite to the first glass container respectively, put 0.04g of selenium powder in it, and pass into nitrogen for 20min to carry out deoxidation, and heat and reflux in a water bath for 60min until the selenium powder is completely dissolved to obtain an aqueous solution of sodium selenosulfite ;
[0023] (2) Add 60mL of deionized water to the second glass container, and carry out deoxidation treatment with nitrogen gas for 30min, then add 0.04g of cadmium chloride to dissolve it completely, then add mercaptoacetic acid of 5 times molar concentration, and use The concentration is 1mol L -1 The pH of the NaOH aqueous solution was adjusted to be 8, and after continuing to feed nitrogen for 40min, an aqueous sodium selenosulfite solution was added, and refluxed in boiling water for 2h to obtain a cadmium selenide nanocrystal solution;
[0024] (3) Add 60 mL of deionized water to the third glass container, pass nitrogen ga...
Embodiment 2
[0026] (1) Add 1 mL of distilled water and 0.1 g of sodium sulfite to the first glass container respectively, place 0.02 g of selenium powder in it, and feed nitrogen gas for 30 min to deoxidize, heat and reflux in a water bath for 30 min until the selenium powder is completely dissolved to obtain an aqueous solution of sodium selenosulfite ;
[0027] (2) Add 40mL of deionized water to the second glass container, and pass nitrogen gas for 20min to carry out deoxidation treatment, then add 0.02g of cadmium chloride to completely dissolve it, and then add mercaptoacetic acid of 5 times molar concentration, Use a concentration of 0.5mol L -1 The pH of the NaOH aqueous solution is adjusted to be 8, and after continuing to feed nitrogen for 30min, an aqueous sodium selenosulfite solution is added, and refluxed in boiling water for 1h to obtain a cadmium selenide nanocrystal solution;
[0028] (3) Add 40 mL of deionized water to the third glass container, ventilate nitrogen for 20 ...
Embodiment 3
[0030] (1) Add 3 mL of distilled water and 0.2 g of sodium sulfite to the first glass container respectively, place 0.05 g of selenium powder in it, and feed nitrogen gas for 40 min to carry out deoxidation, and heat and reflux in a water bath for 90 min until the selenium powder is completely dissolved to obtain an aqueous solution of sodium selenosulfite ;
[0031] (2) Add 80 mL of deionized water to the second glass container, pass nitrogen gas for 40 minutes for deoxidation treatment, then add 0.05 g of cadmium chloride to completely dissolve it, and then add mercaptoethanol with a concentration of 10 times the molar concentration. 2molL -1 The pH of the NaOH aqueous solution is adjusted to be 11, and after continuing to feed nitrogen for 60 minutes, an aqueous sodium selenosulfite solution is added, and refluxed in boiling water for 3 hours to obtain a cadmium selenide nanocrystal solution;
[0032] (3) Add 80 mL of deionized water to the third glass container, pass nitr...
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