A nickel-copper-zinc ferrite and its making method
A technology of nickel-copper-zinc ferrite and its manufacturing method, which is applied in the field of nickel-zinc ferrite and its preparation, and can solve the problem of miniaturization, mobility, integration and multi-functional development of ferrite material electronic equipment, etc. problems, to achieve the effect of excellent microstructure, uniform grain size and wide temperature working range
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Embodiment 1
[0029] Weigh 49.5mol% Fe 2 o 3 , 14.3 mol% NiO, 30.2 mol% ZnO and 6.0 mol% CuO. After mixing the above raw materials, put them into a sand mill and stir them to control the average particle size to 1.00μm±0.20μm. After one spray, pre-fire at 880°C±10°C with an electric rotary kiln. Then the calcined material is put into a sand mill for secondary sand grinding. During the sand grinding process, pure water, dispersant and defoamer are added, and additives are added. Relative to the total amount of the main components, the content of each substance in the additives is The weight percentage content is respectively: V 2 o 5 0.01wt%, MoO 3 0.01wt%, TiO 2 0.02wt%, and the average particle size Φ of the sand mill is controlled to be 1.00μm±0.10μm. Finally, secondary spraying is carried out to obtain nickel-zinc ferrite particle powder.
[0030] Take the granular material and press it into a ring magnetic core of φ25mm×φ15mm×7.5mm, and the molding density is 3.20±0.20g / cm 3 , s...
Embodiment 2
[0033] The composition ratio and process steps are basically the same as in Example 1, and the subcomponents also include MnCO 3 : 0.60wt%, adding in two times, adding 0.45wt% during the first sanding, and adding 0.15wt% during the second sanding.
Embodiment 3
[0035] Weigh 49.0mol% Fe 2 o 3 , 14.6 mol% NiO, 30.4 mol% ZnO and 5.6 mol% CuO. After mixing the above raw materials, put them into a sand mill and stir them to control the average particle size to 1.00μm±0.20μm. After one spraying, pre-fire at 890℃±10℃ with an electric rotary kiln. Then the calcined material is put into a sand mill for secondary sand grinding. During the sand grinding process, pure water, dispersant and defoamer are added, and additives are added. Relative to the total amount of the main components, the content of each substance in the additives is The weight percentage content is respectively: V 2 o 5 0.02wt%, MoO 3 0.018wt%, TiO 2 0.01wt%, Bi 2 o 3 0.02%, the average particle diameter of the control sand mill Φ is 0.95μm±0.1μm. Finally, secondary spraying is carried out to obtain nickel-zinc ferrite particle powder.
[0036] Take the granular material and press it into a ring magnetic core of φ25mm×φ15mm×7.5mm, and the molding density is 3.20±0.20g...
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