Micron nano material composite modified water-based adhesive
A water-based adhesive and nano-modifier technology, applied in the direction of monocarboxylic acid ester copolymer adhesive, adhesive type, hydrocarbon copolymer adhesive, etc., can solve the problem of little improvement and limited effect, etc. question
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[0014] The preparation method of the present invention is as follows: take a certain amount of emulsion and micron-sized powder and mix them fully, and then use them; take a certain amount of nano-sized powder and place them in a certain amount of water, and use ultrasonic waves to fully disperse them until they are transparent, and become Nano-modifier dispersion; then take a certain amount of dispersed nano-modifier dispersion and add it to the mixture of micron-sized powder and emulsion, stir thoroughly, and finally obtain the micron-nano modified water-based adhesive.
[0015] The adhesive matrix is selected from at least one emulsion that can be used as an adhesive, preferably polyvinyl acetate emulsion, polyurethane emulsion, polyvinyl acetate-vinyl emulsion and acrylic emulsion.
[0016] Micron-sized inorganic powder modifiers are preferably calcium carbonate powder, quartz powder, talc powder, mica powder, silicon carbide powder and corundum powder.
[0017] The pref...
Embodiment 1
[0021] Embodiment 1: prepare the water-based adhesive modified by talcum powder and nano-calcium carbonate
[0022] Weigh 83.18g of polyvinyl acetate emulsion and 18.01g of talcum powder with a balance, stir well, and set aside. Take 12.4g of a dispersion liquid containing 5% of nano-barium sulfate powder and add it into the mixture of emulsion and talcum powder, and stir thoroughly to obtain a water-based adhesive modified by talc powder and nano-barium sulfate with excellent performance.
[0023] The preparation method of nano-barium sulfate aqueous dispersion is as follows: the nano-barium sulfate powder and water are oscillated and dispersed under the action of 28KHz ultrasonic waves in a container at a mass ratio of 5:95, and prepared into a uniform transparent or Translucent dispersion.
Embodiment 2
[0025] Weigh 80.33g of acrylic acid emulsion and 23.72g of calcium carbonate micropowder with a balance, stir well, and set aside. Take 15g of a dispersion liquid containing 6% of nano-silica powder and add it to the mixture of acrylic acid emulsion and calcium carbonate micropowder, and stir thoroughly to obtain a water-based adhesive modified by micron and nanometer powders with good performance.
[0026] The preparation method of the nano-silica aqueous dispersion is as follows: the nano-silica powder and water are oscillated and dispersed under the action of ultrasonic waves in a container at a ratio of 6:94 by mass, and prepared into a uniform transparent dispersion after 30-60 minutes. or translucent dispersions.
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