Paederia extractive and medical use of the same
A kind of extract, the technology of chicken dung vine, which is applied in the field of chicken dung rattan extract, can solve the problems of poor analgesic effect and unstable effect, and achieve excellent anti-inflammatory and analgesic effects without addiction
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0027] Embodiment 1 prepares the extract of chicken dung vine
[0028] 1. 1 kg of washed and broken whole herb of Caulis chinensis was reflux extracted with 70% ethanol solution for 2 hours, collected the ethanol solution and concentrated it to dryness under reduced pressure to obtain 90 grams of extract;
[0029] 2. Dissolve the extract obtained in step 1 with 2 liters of ethanol solution with a volume concentration of 10% at a temperature of 45° C., then centrifuge the resulting solution and get the supernatant;
[0030] 3. the gained supernatant is passed through the macroporous adsorption resin chromatography column, and the weight of the macroporous adsorbent resin is 20 times of the obtained extract weight;
[0031] 4. Wash the macroporous adsorption resin column with a volume concentration of 20% ethanol solution until the color of the solution becomes light. The amount of ethanol used is 10 times the volume of the macroporous adsorption resin column; its flow rate is ...
Embodiment 2
[0035] Embodiment 2 prepares the extract of chicken dung vine
[0036] Repeat the extraction steps of Example 1, but the ethanol concentration of the original step 1, the concentration of the ethanol solution used to dissolve the medicinal extract of the step 2, the amount of the macroporous adsorption resin of the step 3, the amount of the macroporous adsorption resin used for the washing and adsorption of the steps 4 and 5 The concentration of the ethanol solution of column and consumption and the flow velocity when washing column thereof are changed to respectively: 90%; 5%; 30 times; 25%; 8 times; 70%; 15 times; 1.5;); The weight of the extract of gained It is 11g, and the content of gallizine and gallizine in the extract is 20% and 70%, respectively.
Embodiment 3
[0037] Embodiment 3 prepares the extract of chicken dung vine
[0038] Repeat the extraction steps of Example 1, but the ethanol concentration of the original step 1, the concentration of the ethanol solution used to dissolve the medicinal extract of the step 2, the amount of the macroporous adsorption resin of the step 3, the amount of the macroporous adsorption resin used for the washing and adsorption of the steps 4 and 5 The concentration of the ethanol solution of column and consumption and the flow velocity when washing column thereof are changed into respectively: (50%; 3%; 35 times; 15%; 12 times; 80%; 20 times; 2); The weight of the extract of gained It is 12g, and the content of gallizine and gallizine in the extract is 65% and 20%, respectively.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com