Method for activating membrane electrode of fuel cell
A fuel cell membrane and fuel cell technology, which is applied to fuel cells, fuel cell components, battery electrodes, etc., can solve the problems of low fuel cell power and long activation time.
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Embodiment 1
[0037] This example illustrates the activation method of the fuel cell membrane electrode provided by the present invention
[0038] 1. Preparation and initial performance test of membrane electrode
[0039] (1) Mix 0.2 parts by weight of carbon black (Vulcan XC72R, Cabot), 0.1 parts by weight of PTFE emulsion (FR303A, Shanghai Sanaifu New Material Co., Ltd.) with a solid content of 60% by weight, and 10 parts by weight of deionized water , Ultrasonic dispersion for 30 minutes to obtain a carbon dispersion, and then the carbon dispersion is coated on carbon paper (TGP-H-90, Toray company), after drying at 100 ℃, the weight of the carbon paper is 1 mg / cm 2 , Then placed in a high temperature oven at 350°C for 20 minutes to obtain a gas diffusion layer;
[0040] (2) 0.2 parts by weight of Pt / C catalyst (Hispec8100, product of Johnson Matthey) and 2 parts by weight of nafion dispersion (DE520, product of DUPONT) with a platinum loading of 47.7% by weight are mixed uniformly. The cata...
Embodiment 2
[0049] This example illustrates the activation method of the fuel cell membrane electrode provided by the present invention
[0050] 1. Preparation and initial performance test of membrane electrode
[0051] (1) Mix 0.2 parts by weight of carbon black (Vulcan XC72R, Cabot), 0.1 parts by weight of PTFE emulsion (FR303A, Shanghai Sanaifu New Material Co., Ltd.) with a solid content of 60% by weight, and 10 parts by weight of deionized water, Disperse ultrasonically for 30 minutes to obtain a carbon dispersion, and then coat the carbon dispersion on carbon paper (TGP-H-90, Toray). After drying at 100°C, the carbon paper gains 1 mg / cm 2 , Then placed in a high temperature oven at 350°C for 20 minutes to obtain a gas diffusion layer;
[0052] (2) 0.2 parts by weight of Pt / C catalyst (Hispec8100, product of Johnson Matthey) and 2 parts by weight of nafion dispersion (DE520, product of DUPONT) were mixed uniformly with a platinum loading amount of 47.7% by weight. The catalyst dispersion...
Embodiment 3
[0061] This example illustrates the activation method of the organic fuel cell membrane electrode provided by the present invention
[0062] 1. Preparation and initial performance test of membrane electrode
[0063](1) Mix 0.2 parts by weight of carbon black (Vulcan XC72R, Cabot), 0.06 parts by weight of PTFE emulsion (FR303A, Shanghai Sanaifu New Material Co., Ltd.) with a solid content of 60% by weight, and 10 parts by weight of deionized water, Disperse ultrasonically for 30 minutes to obtain a carbon dispersion, and then coat the carbon dispersion on carbon paper (TGP-H-90, Toray). After drying at 100°C, the carbon paper gains 1 mg / cm 2 , Then placed in a high temperature oven at 350°C for 20 minutes to obtain a gas diffusion layer;
[0064] (2) 0.5 parts by weight of Pt / Ru black catalyst (Hispec6000, product of Johnson Matthey) and 15 parts by weight of nafion dispersion (DE520, product of DUPONT) are mixed uniformly. Ultrasonic dispersion to obtain a catalyst dispersion, and...
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