Composite cellulose viscose filament yarn with composite cellulose pulp as raw materials made of wood and bamboo mixture and preparation method thereof
A technology of composite cellulose and viscose filament, which is applied in the direction of cellulose/protein conjugated rayon, chemical post-processing of fibers, plant raw materials, etc., can solve the problems of low production efficiency and high cost, and achieve low cost, Production process optimization, glossy effect
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Embodiment 1
[0035] Production of 120D / 30F composite cellulose viscose filament:
[0036] Raw materials: mix natural wood and bamboo raw materials to make new composite cellulose pulp, wherein the weight ratio of wood and bamboo raw materials is: 50%:50%.
[0037] Dipping process:
[0038] Alkaline temperature: 35°C
[0039] Alkaline concentration: 188g / l
[0040] Dipping time: 100 minutes
[0041] Alkali fiber composition: α-cell content: 28%
[0042] NaOH content: 16.3%
[0043] Amount of VIF-64 added: 0.5% (for α-cell)
[0044] Amount of VIF-9 added: 1.0% (for α-cell)
[0045] Yellowing process:
[0046] CS 2 Added amount: 35.5% (for α-cell)
[0047] Yellowing temperature: 30°C
[0048] Yellowing time: 70 minutes
[0049] Dissolving temperature: 8°C
[0050] Addition of VIF-51 / 41: 2.0% (for α-cell) Viscose before spinning:
[0051] α-cell content: 7.85%
[0052] NaOH content: 6.12%
[0053] Viscosity (falling ball met...
Embodiment 2
[0079] Production of 600D / 100F composite cellulose viscose filament:
[0080] Raw materials: mix natural wood and bamboo raw materials to make new composite cellulose pulp, wherein the weight ratio of wood and bamboo raw materials is: 80%: 20%.
[0081] Dipping process:
[0082] Alkaline temperature: 48°C
[0083] Alkaline concentration: 180g / l
[0084] Dipping time: 80 minutes
[0085] Alkali fiber composition: α-cell content: 32.3%
[0086] NaOH content: 15.8%
[0087] Amount of VIF-64 added: 1.0% (for α-cell)
[0088] The amount of VIF-9 added: 1.3% (for α-cell)
[0089] Yellowing process:
[0090] CS 2 Added amount: 30.5% (for α-cell)
[0091] Yellowing temperature: 26.5°C
[0092] Yellowing time: 80 minutes
[0093] Dissolving temperature: 13°C
[0094] Addition amount of VIF-51 / 41: 1.5% (for α-cell)
[0095] Viscose before spinning:
[0096] α-cell content: 8.03%
[0097] NaOH content: 5.98%
...
Embodiment 3
[0124]Production of 120D / 30F dull composite cellulose viscose filament:
[0125] The new composite cellulose pulp is prepared by mixing natural wood and bamboo raw materials, wherein the weight ratio of the wood and bamboo raw materials is 20%:80%.
[0126] Dipping process:
[0127] Alkaline temperature: 42°C
[0128] Alkaline concentration: 216g / l
[0129] Dipping time: 90 minutes
[0130] Alkali fiber composition: α-cell content: 29.6%
[0131] NaOH content: 16.3%
[0132] Amount of VIF-64 added: 1.2% (for α-cell)
[0133] Amount of VIF-9 added: 1.0% (for α-cell)
[0134] Yellowing process:
[0135] CS 2 Added amount: 28.5% (for α-cell)
[0136] Yellowing temperature: 31°C
[0137] Yellowing time: 45 minutes
[0138] Dissolving temperature: 15°C
[0139] Addition amount of VIF-51 / 41: 1.5% (for α-cell)
[0140] Viscose before spinning:
[0141] α-cell content: 7.85%
[0142] NaOH content: 5.96%
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