Shenmai fibrous root polysaccharide granules as well as preparation method and application thereof
The technology of granules and fibrous roots is applied in the field of ginseng fibrous root polysaccharide granules and its preparation, which can solve the problems of waste, environmental burden and the like, and achieve the effects of convenient instrument, low cost and lower production cost.
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[0028] A preparation method of ginseng root polysaccharide granules of the present invention comprises the following steps:
[0029] ①Ethanol impurity removal: ginseng fibrous roots and Ophiopogon japonicus fibrous roots are respectively added to ethanol for impregnation, then heated and refluxed for extraction, after the fibrous roots are recovered, dried in a desiccator to prepare the impurity-removed ginseng fibrous roots and Ophiopogon japonicus fibrous roots;
[0030] ②Water extraction and concentration: Mix the fibrous roots of ginseng and Ophiopogon japonicus according to the mass ratio of 1:1-1:9 (w / w) after removing impurities, add distilled water for extraction, and extract twice; 1 / 20 volume, filtered, and the concentrate was prepared for use;
[0031] ③Alcohol precipitation: add absolute ethanol to the concentrate prepared in step ②, let stand at 4°C for 12 hours, collect the precipitate by centrifugation, wash the precipitate with absolute ethanol and acetone in t...
Embodiment 1
[0051] A kind of ginseng fibrous root polysaccharide granules, prepared according to the following method:
[0052] ①Ethanol impurity removal: 100g ginseng fibrous root and 900g Ophiopogon japonicus fibrous root were respectively soaked in 90% (V / V) ethanol for 2 hours, then heated with an electric heating mantle to keep them in a slightly boiling state at 100°C for 3 times of heating and reflux extraction. 10 times the amount of 90% (V / V) ethanol was used for reflux extraction for 2h; fibrous roots were recovered and dried in a desiccator; ginseng fibrous roots and Ophiopogon japonicus fibrous roots after impurity removal were prepared;
[0053] ②Water extraction and concentration: The fibrous roots of ginseng and Ophiopogon japonicus are mixed according to the mass ratio of 1:9 (w / w) after removing impurities, and distilled water is added for extraction. The total mass of ginseng fibrous root and Ophiopogon japonicus fibrous root and distilled water were extracted twice, 2h ...
Embodiment 2
[0058] A kind of ginseng fibrous root polysaccharide granules, prepared according to the following method:
[0059] ①Ethanol impurity removal: 100g of ginseng fibrous root and 900g of Ophiopogon japonicus fibrous root were soaked in ethanol with a volume fraction of 70% (V / V) for 2 hours, and heated with an electric heating mantle to keep them in a slightly boiling state at 100 °C for heating and reflux extraction. 3 times, using 8 times the amount of 70% (V / V) ethanol for reflux extraction for 2.5h each time; reclaiming fibrous roots, drying in a desiccator; preparing the ginseng fibrous roots and Ophiopogon japonicus fibrous roots after removing impurities;
[0060] ②Water extraction and concentration: The fibrous roots of ginseng and Ophiopogon japonicus are mixed according to the mass ratio of 1:9 (w / w) after removing impurities, and distilled water is added for extraction. The total mass of ginseng fibrous root and Ophiopogon japonicus fibrous root and distilled water are...
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