Pressure-sensitive adhesive composition and preparation method thereof
A technology of pressure-sensitive adhesives and compositions, applied in the direction of adhesive additives, adhesive types, ester copolymer adhesives, etc., can solve the problems of pressure-sensitive adhesives such as reduced viscosity when exposed to moisture
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Embodiment 1
[0021] A pressure-sensitive adhesive composition, which takes the following raw materials:
[0022] Acrylate 600g;
[0023] Acrylic acid 200g;
[0024] Ethyl salicylate 90g;
[0025] Acetate starch 50g;
[0026] Sodium alginate 30g;
[0027] Anhydrous isopropanol 220g;
[0028] Aziridine 20g;
[0029] Polyethylene glycol 60g.
[0030] Preparation of pressure-sensitive adhesive composition: 1) Add anhydrous isopropanol into the reaction kettle, heat to 68-80°C, add acrylate and acrylic acid, mix well to obtain a mixed solution; 2) use the mixed solution in step 1) Add aziridine and polyethylene glycol to the mixture, and continue to heat to 90-102°C for cross-linking reaction; 3) Continue to add ethyl salicylate, acetate starch and sodium alginate, stir evenly, after the isopropanol volatilizes, The pressure-sensitive adhesive composition of Example 1 was obtained.
Embodiment 2
[0032] A pressure-sensitive adhesive composition, which takes the following raw materials:
[0033] Acrylate 620g;
[0034] Acrylic acid 300g;
[0035] Ethyl salicylate 60g;
[0036] Acetate starch 80g;
[0037] Sodium alginate 60g;
[0038] Anhydrous isopropanol 250g;
[0039] Aziridine 50g;
[0040] Polyethylene glycol 100g.
[0041] Preparation of pressure-sensitive adhesive composition: 1) Add anhydrous isopropanol into the reaction kettle, heat to 68-80°C, add acrylate and acrylic acid, mix well to obtain a mixed solution; 2) use the mixed solution in step 1) Add aziridine and polyethylene glycol to the mixture, and continue to heat to 90-102°C for cross-linking reaction; 3) Continue to add ethyl salicylate, acetate starch and sodium alginate, stir evenly, after the isopropanol volatilizes, The pressure-sensitive adhesive composition of Example 2 was obtained.
Embodiment 3
[0043] A pressure-sensitive adhesive composition, which takes the following raw materials:
[0044] Acrylate 650g;
[0045] Acrylic acid 280g;
[0046] Ethyl salicylate 80g;
[0047] Acetate starch 60g;
[0048] Sodium alginate 50g;
[0049] Anhydrous isopropanol 270g;
[0050] Aziridine 40g;
[0051] Polyethylene glycol 80g.
[0052] Preparation of pressure-sensitive adhesive composition: 1) Add anhydrous isopropanol into the reaction kettle, heat to 68-80°C, add acrylate and acrylic acid, mix well to obtain a mixed solution; 2) use the mixed solution in step 1) Add aziridine and polyethylene glycol to the mixture, and continue to heat to 90-102°C for cross-linking reaction; 3) Continue to add ethyl salicylate, acetate starch and sodium alginate, stir evenly, after the isopropanol volatilizes, The pressure-sensitive adhesive composition of Example 3 was obtained.
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