Desulfurization method of waste tire rubber powder
A technology of waste tire rubber and desulfurized rubber, which is applied in the field of recycled rubber, can solve the problems of breaking rubber macromolecular chains, simultaneous opening of double bonds, and high processing temperature, so as to achieve environmental protection in the desulfurization process, increase sol content, and reduce crosslinking density Effect
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Embodiment 1
[0027] This embodiment provides a method for desulfurizing waste tire rubber powder, said method comprising the following steps:
[0028] Step S1, add 100 parts by weight of waste tire rubber powder and 10 parts by weight of furfural oil extracted into the airtight container, mix uniformly at room temperature, then add 5 parts by weight of lauryl mercaptan and 5 parts by weight of lauric acid, mix uniformly, Get the primary mix.
[0029] In step S2, the temperature of the primary mixture obtained in step S1 is raised to 100° C., and the mixture is stirred at a high speed of 600 rad / min for 30 minutes to obtain a mixed rubber material.
[0030] Step S3, finally melt and extrude the mixed compound prepared in step S2 with a conical twin-screw extruder, control the screw speed to 80rad / min, the barrel temperature to 220°C, the extrusion time to 15min, and pelletize after extrusion, complete Desulfurization process of waste tire rubber powder to obtain desulfurized rubber.
Embodiment 2
[0032] This embodiment provides a method for desulfurizing waste tire rubber powder, said method comprising the following steps:
[0033] Step S1, add 100 parts by weight of waste tire rubber powder and 8 parts by weight of furfural oil extracted into the airtight container, mix uniformly at room temperature, then add 8 parts by weight of lauryl mercaptan and 8 parts by weight of lauric acid, mix uniformly, Get the primary mix.
[0034] In step S2, the temperature of the primary mixture obtained in step S1 is raised to 95° C., and the mixture is stirred at a high speed of 600 rad / min for 30 minutes to obtain a mixed rubber material.
[0035] Step S3, finally melt and extrude the mixed rubber material prepared in step S2 with a conical twin-screw extruder, control the screw speed at 90rad / min, the barrel temperature at 220°C, the extrusion time for 15min, and pelletize after extrusion, complete Desulfurization process of waste tire rubber powder to obtain desulfurized rubber. ...
Embodiment 3
[0037] This embodiment provides a method for desulfurizing waste tire rubber powder, said method comprising the following steps:
[0038] Step S1, add 100 parts by weight of waste tire rubber powder and 10 parts by weight of furfural oil extracted into the airtight container, mix uniformly at room temperature, then add 8 parts by weight of lauryl mercaptan and 8 parts by weight of lauric acid, mix uniformly, Get the primary mix.
[0039] In step S2, the temperature of the primary mixture obtained in step S1 is raised to 90° C., and the mixture is stirred at a high speed of 600 rad / min for 30 minutes to obtain a mixed rubber material.
[0040] Step S3, finally melt and extrude the mixed rubber material prepared in step S2 with a conical twin-screw extruder, control the screw speed at 100rad / min, the barrel temperature at 220°C, the extrusion time for 15min, and pelletize after extrusion, complete Desulfurization process of waste tire rubber powder to obtain desulfurized rubber...
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