Concrete inner surface hydrophobic treatment agent and preparation method thereof
A hydrophobic treatment and concrete internal technology, which is applied in the field of concrete inner surface hydrophobic treatment agent and its preparation, can solve the problems of insufficient durability and high cost, and achieve the effect of high labor intensity, high production cost, convenient transportation and use
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Embodiment 1
[0051] 1) Use prenol polyoxyethylene ether (TPEG) with a molecular weight of 2400, according to TPEG: hydroxyethyl acrylate: hydrogen peroxide (concentration 27.5%): vitamin C: thioglycolic acid: water = 350: 80: 3: 0.3: 0.4 : The mass ratio of 425 synthesizes the coating solution;
[0052] The synthesis steps are:
[0053] First add 350 parts of prenol polyoxyethylene ether and 300 parts of deionized water into a three-necked flask, and stir at room temperature for 20 minutes to ensure that the prenol polyoxyethylene ether is completely dissolved;
[0054] Add 3 parts of hydrogen peroxide (concentration 27.5%) and stir for 5 minutes;
[0055] Prepare liquid A and liquid B. Among them, liquid A: 0.4 parts of thioglycolic acid, 0.3 parts of vitamin C, and 85 parts of deionized water. Liquid B: 80 parts of hydroxyethyl acrylate, 40 parts of deionized water;
[0056] Both liquid A and liquid B were added dropwise into the three-necked flask, wherein liquid A was added dropwis...
Embodiment 2
[0078] 1) Prenol polyoxyethylene ether (TPEG) with a molecular weight of 3000 is used, according to TPEG: hydroxybutyl acrylate: ammonium persulfate: ferrous sulfate heptahydrate: mercaptopropionic acid: water = 330: 100: 2: 0.2: 0.3:435 mass ratio, the coating solution is synthesized;
[0079] The synthesis steps are,
[0080] First add 330 parts of prenol polyoxyethylene ether and 310 parts of deionized water into a three-necked flask, and stir for 20 minutes at room temperature to ensure that the prenol polyoxyethylene ether is completely dissolved; add 2 parts of ammonium persulfate and stir for 5 minute;
[0081] Prepare liquid A and liquid B. Wherein, liquid A: 0.3 parts of thioglycolic acid, 0.2 parts of ferrous sulfate, and 85 parts of deionized water. Liquid B: 100 parts of hydroxybutyl acrylate, 40 parts of deionized water;
[0082] Both liquid A and liquid B are added dropwise into the three-necked flask, wherein liquid A is added dropwise for 3 hours, and liqui...
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