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Production process of feed-grade manganese glutamate

A technology of manganese glutamate and production process, applied in the field of production technology of feed-grade manganese glutamate, can solve problems such as being difficult to apply to actual production, and achieve the effects of low equipment cost, few components and easy maintenance

Pending Publication Date: 2021-12-28
GUANGHAN LONGDA FEED
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, the existing production techniques for the synthesis of manganese glutamate are limited to laboratory synthesis and are difficult to apply to actual production. Therefore, a production technique for feed grade manganese glutamate is proposed

Method used

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  • Production process of feed-grade manganese glutamate
  • Production process of feed-grade manganese glutamate
  • Production process of feed-grade manganese glutamate

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] see Figure 1-3 :

[0026] (1) Open the cover plate 4 to feed the material to the feed port 3, first add deionization;

[0027] (2) Add feed grade glutamic acid then, ventilate to vent pipe 5, gas overflows along pore 7, produces air flow in the material in reactor 1, plays stirring effect to material, and reactor 1 is warmed up to 55 ℃ during stirring process. ℃, slowly add manganese sulfate, the connecting pipe 8 is connected to the reaction kettle 1, and the materials in the reaction kettle 1 enter the connecting pipe 8 at the same time. During the process of adding manganese sulfate, use the sampler 9 to insert into the connecting pipe 8 to extract the reaction kettle 1. For materials, detect the manganese sulfate content and glutamic acid content in the material, and control the molar ratio of the total manganese sulfate content to glutamic acid to be 1:1;

[0028] (3) After the feeding is completed, continue to heat up, control the reaction temperature to 75°C, ...

Embodiment 2

[0036] see Figure 1-3 :

[0037] (1) Open the cover plate 4 to feed the material to the feed port 3, first add deionization;

[0038] (2) Add feed grade glutamic acid then, ventilate to ventilation pipe 5, gas overflows along pore 7, produces air flow in the material in reactor 1, plays stirring effect to material, and reactor 1 is warmed up to 60 ℃ during stirring process ℃, slowly add manganese sulfate, the connecting pipe 8 is connected to the reaction kettle 1, and the materials in the reaction kettle 1 enter the connecting pipe 8 at the same time. During the process of adding manganese sulfate, use the sampler 9 to insert into the connecting pipe 8 to extract the reaction kettle 1. For materials, detect the manganese sulfate content and glutamic acid content in the material, and control the molar ratio of the total manganese sulfate content to glutamic acid to be 1:1;

[0039] (3) After the feeding is completed, continue to heat up, control the reaction temperature to ...

Embodiment 3

[0047] see Figure 1-3 :

[0048] (1) Open the cover plate 4 to feed the material to the feed port 3, first add deionization;

[0049] (2) Add feed grade glutamic acid then, ventilate to vent pipe 5, gas overflows along pore 7, produces airflow in the material in reactor 1, plays stirring effect to material, and reactor 1 is warmed up to 65 ℃ in stirring process. ℃, slowly add manganese sulfate, the connecting pipe 8 is connected to the reaction kettle 1, and the materials in the reaction kettle 1 enter the connecting pipe 8 at the same time. During the process of adding manganese sulfate, use the sampler 9 to insert into the connecting pipe 8 to extract the reaction kettle 1. For materials, detect the manganese sulfate content and glutamic acid content in the material, and control the molar ratio of the total manganese sulfate content to glutamic acid to be 1:1;

[0050] (3) After the feeding is completed, continue to heat up, control the reaction temperature to 85°C, and k...

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Abstract

The invention relates to the technical field of production of manganese glutamate, and particularly discloses a production process of feed-grade manganese glutamate. The process adopts a wet synthesis process and comprises the following steps: reacting manganese sulfate with glutamic acid in a solution to obtain a manganese glutamate solution by controlling the reaction temperature and the reaction time, cooling and crystallizing to obtain a manganese glutamate product, performing drying to remove surface moisture, and then screening to remove large-particle products so as to obtain the feed-grade manganese glutamate. The process is low in energy consumption, green and environment-friendly, and does not generate substances polluting the environment, and various indexes such as the product content and heavy metals can meet the quality requirements of the feed-grade manganese glutamate; as only heating and stirring are needed in the production process, complex operations such as ultrasonic are not needed, and the equipment cost is low; the synthesis process is carried out in water, no harmful by-product is generated, mother liquor can be recycled, organic solvent extraction is not needed, the process is green and environment-friendly, post-treatment is simple, and no three wastes are generated; and the synthesis process is environment-friendly, economical and efficient.

Description

technical field [0001] The invention relates to the technical field of manganese glutamate production, and the specific field is the production process of feed-grade manganese glutamate. Background technique [0002] Manganese plays an important role in the growth of animal bones. Although the proportion of manganese in the animal body is very small, it is closely related to the development of animal bones. Manganese plays a very important role in the development of animal bones. Manganese Elements affect the normal growth and development of animal bones, mainly because manganese participates in the formation of chondroitin sulphate, which constitutes the bone matrix. Chondroitin Sulphate is a constituent of organic mucopolysaccharides. Manganese is also an essential trace element in the synthesis of polysaccharide polymerase and galactosyltransferase in animals. If the animal is growing, the lack of manganese may cause the activities of polysaccharide polymerase and galac...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C227/18C07C227/42C07C229/76B01F13/02B01J19/00B01J19/24B01F33/40
CPCC07C227/18C07C227/42B01J19/0053B01J19/24C07C229/76
Inventor 李家军邵勇杰吴兵李凤仙吕程
Owner GUANGHAN LONGDA FEED
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