Porous aerogel material, preparation method thereof and electronic cigarette atomization core
A technology of porous airgel and airgel powder, which is applied in the field of electronic cigarettes, can solve the problems of insufficient oil storage of electronic cigarette cores, uneven distribution of e-liquid and heating, over-burning atomization, etc., to achieve low density and high supply Smooth, anti-odor effect
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[0028] The present invention also provides a method for preparing the porous airgel material described in the above technical solution, comprising the following steps:
[0029] a) mixing silica airgel powder and pore-forming agent powder to obtain a mixed powder;
[0030] b) placing the mixed powder in a mould, and compacting to obtain a semi-finished product;
[0031] c) heating the semi-finished product to obtain a porous airgel material.
[0032] In the preparation method provided by the present invention, in step a), the relevant information of the silica airgel powder and pore-forming agent powder has been introduced above, and will not be repeated here; the stirring speed of the mixing is preferably 20~200r / min, specifically 20r / min, 30r / min, 40r / min, 50r / min, 60r / min, 70r / min, 80r / min, 90r / min, 100r / min, 110r / min, 120r / min, 130r / min, 140r / min, 150r / min, 160r / min, 170r / min, 180r / min, 190r / min or 200r / min; the mixing time is preferably 5-30min, specifically 5min, 7min,...
Embodiment 1
[0040] A porous airgel material that can be applied to the preparation of electronic smog cores is made of silica airgel with a mass fraction of 70wt% and polymethyl methacrylate (PMMA) with a mass fraction of 70wt% by mixing, stirring, Prepared by pressing and heating. Among them, the silica airgel powder used is purchased from Anhui Keang Nano Technology Co., Ltd., the brand KNF-W, its thermal conductivity is 0.017~0.023W / (m·K), and its density is 0.1g / cm 3 , with a pore size of 15nm, a porosity of 90%, and a particle size of 15 μm; the polymethylmethacrylate (PMMA) pore-forming agent powder used is monodisperse, with an average particle size of 20 μm, purchased from Soken Chemical (Suzhou) Co., Ltd. Company, brand MX1500HF.
[0041] The preparation method of the above-mentioned porous airgel material specifically comprises the following steps:
[0042] Step 1: Weigh a certain mass of silica airgel powder and polymethyl methacrylate (PMMA) powder according to the mass rati...
Embodiment 2
[0049] A porous airgel material that can be applied to the preparation of electronic smoke cores is composed of silica airgel with a mass fraction of 60wt%, 30wt% polymethyl methacrylate (PMMA) and 10wt% carbonic acid Ammonium Hydrogen (NH 4 CO 3 ) are prepared by mixing, stirring, compacting and heating. Among them, the silica airgel powder used is purchased from Anhui Keang Nano Technology Co., Ltd., the brand KNF-W, its thermal conductivity is 0.017~0.023W / (m·K), and its density is 0.1g / cm 3 , the pore size is 15nm, the porosity is 90%, and the particle size is 15 μm; the polymethyl methacrylate (PMMA) pore-forming agent powder is monodisperse, and the average particle size is 20 μm, purchased from Zongyan Chemical (Suzhou) Co., Ltd. , grade MX1500HF; ammonium bicarbonate (NH 4 CO 3 ) with an average particle size of 3 mm.
[0050] The preparation method of the above-mentioned porous airgel material specifically comprises the following steps:
[0051] Step 1: Weigh a ...
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