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Porous aerogel material, preparation method thereof and electronic cigarette atomization core

A technology of porous airgel and airgel powder, which is applied in the field of electronic cigarettes, can solve the problems of insufficient oil storage of electronic cigarette cores, uneven distribution of e-liquid and heating, over-burning atomization, etc., to achieve low density and high supply Smooth, anti-odor effect

Pending Publication Date: 2021-12-03
UNIV OF SCI & TECH OF CHINA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In view of this, the object of the present invention is to provide a porous airgel material and its preparation method and electronic smog core. The material provided by the present invention realizes the combination of artificially manufactured pores and the micropores of the material itself, which can effectively solve the problem of electronic smog. Insufficient oil storage in the cartridge, uneven heating of the e-liquid distribution, over-burning and insufficient atomization, etc.

Method used

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Examples

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Effect test

preparation example Construction

[0028] The present invention also provides a method for preparing the porous airgel material described in the above technical solution, comprising the following steps:

[0029] a) mixing silica airgel powder and pore-forming agent powder to obtain a mixed powder;

[0030] b) placing the mixed powder in a mould, and compacting to obtain a semi-finished product;

[0031] c) heating the semi-finished product to obtain a porous airgel material.

[0032] In the preparation method provided by the present invention, in step a), the relevant information of the silica airgel powder and pore-forming agent powder has been introduced above, and will not be repeated here; the stirring speed of the mixing is preferably 20~200r / min, specifically 20r / min, 30r / min, 40r / min, 50r / min, 60r / min, 70r / min, 80r / min, 90r / min, 100r / min, 110r / min, 120r / min, 130r / min, 140r / min, 150r / min, 160r / min, 170r / min, 180r / min, 190r / min or 200r / min; the mixing time is preferably 5-30min, specifically 5min, 7min,...

Embodiment 1

[0040] A porous airgel material that can be applied to the preparation of electronic smog cores is made of silica airgel with a mass fraction of 70wt% and polymethyl methacrylate (PMMA) with a mass fraction of 70wt% by mixing, stirring, Prepared by pressing and heating. Among them, the silica airgel powder used is purchased from Anhui Keang Nano Technology Co., Ltd., the brand KNF-W, its thermal conductivity is 0.017~0.023W / (m·K), and its density is 0.1g / cm 3 , with a pore size of 15nm, a porosity of 90%, and a particle size of 15 μm; the polymethylmethacrylate (PMMA) pore-forming agent powder used is monodisperse, with an average particle size of 20 μm, purchased from Soken Chemical (Suzhou) Co., Ltd. Company, brand MX1500HF.

[0041] The preparation method of the above-mentioned porous airgel material specifically comprises the following steps:

[0042] Step 1: Weigh a certain mass of silica airgel powder and polymethyl methacrylate (PMMA) powder according to the mass rati...

Embodiment 2

[0049] A porous airgel material that can be applied to the preparation of electronic smoke cores is composed of silica airgel with a mass fraction of 60wt%, 30wt% polymethyl methacrylate (PMMA) and 10wt% carbonic acid Ammonium Hydrogen (NH 4 CO 3 ) are prepared by mixing, stirring, compacting and heating. Among them, the silica airgel powder used is purchased from Anhui Keang Nano Technology Co., Ltd., the brand KNF-W, its thermal conductivity is 0.017~0.023W / (m·K), and its density is 0.1g / cm 3 , the pore size is 15nm, the porosity is 90%, and the particle size is 15 μm; the polymethyl methacrylate (PMMA) pore-forming agent powder is monodisperse, and the average particle size is 20 μm, purchased from Zongyan Chemical (Suzhou) Co., Ltd. , grade MX1500HF; ammonium bicarbonate (NH 4 CO 3 ) with an average particle size of 3 mm.

[0050] The preparation method of the above-mentioned porous airgel material specifically comprises the following steps:

[0051] Step 1: Weigh a ...

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Abstract

The invention belongs to the field of electronic cigarettes, and particularly relates to a porous aerogel material, a preparation method thereof and an electronic cigarette atomization core. The porous aerogel material provided by the invention is prepared by mixing silicon dioxide aerogel powder and pore-forming agent powder, pressing and heating, wherein the pore-forming agent powder comprises one or more of ammonium bicarbonate, ammonium oxalate and polymethyl methacrylate; the particle size of the pore-forming agent powder is larger than the pore diameter of the silicon dioxide aerogel powder. The porous aerogel material provided by the invention has the advantages of reasonable porosity, large specific surface area, small density and high temperature resistance through combination of nano micropores of the silicon dioxide aerogel and artificial pores. The atomization core of the electronic cigarette prepared from the material is smooth in tobacco tar supply, and can adjust the dryness and humidity of a local area, so that atomized smoke is finer and smoother; and moreover, the material has excellent temperature resistance and heat insulation performance, so that the safe use of equipment can be ensured, and peculiar smell spreading caused by high-temperature carbonization generated by over-fast local heating of the tobacco tar can be prevented.

Description

technical field [0001] The invention belongs to the field of electronic cigarettes, and in particular relates to a porous airgel material, a preparation method thereof, and an electronic cigarette core. Background technique [0002] At present, the global control over traditional tobacco products is increasing year by year, and people pay more attention to their own health, which makes new tobacco products receive more attention. Especially e-cigarettes, because they can reduce the release of harmful components, have gradually become an important development direction and research and development hotspot of new tobacco products. [0003] E-cigarettes are electronic products that mimic cigarettes and have the same look, smoke, taste and feel as cigarettes. It is a product that is powered by a rechargeable lithium polymer battery to drive the atomizer. By heating the e-liquid in the oil tank, it turns nicotine into vapor for users to smoke. [0004] The electronic cigarette ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B30/00C04B38/06C04B38/02C04B38/08A24F40/40A24F40/10A24F40/70C04B14/06
CPCC04B30/00C04B38/067C04B38/02A24F40/40A24F40/10A24F40/70C04B2201/32C04B14/064C04B24/2641C04B22/10C04B38/0051
Inventor 吴长征谢毅
Owner UNIV OF SCI & TECH OF CHINA
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