A method for removing a variety of harmful substances in capsanthin
A technology of capsanthin and harmful substances, which is applied in the field of extraction of natural products, can solve the problems of pigment loss, high temperature, and different adsorption effects, and achieve the effects of improved safety, less loss, and simple operation
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Embodiment 1
[0038] The present embodiment relates to the removal of harmful components in capsanthin, including the following steps:
[0039] Dissolve 1000 g of capsanthin (color value 145.2, benzopyrene 26 ppb, total Sudan red (Sudan red I-IV) 200 ppb, rhodamine B 65 ppb, ethion 36 ppm, chlorpyrifos 12 ppm, triazophos 21 ppm) into vegetable oil. Mixed solution of extraction solvent and acetone (vegetable oil extraction solvent: acetone=3:2) 10000ml, filter to remove solid insolubles, put the feed liquid into the feed tank of organic solvent-resistant nanofiltration membrane equipment, turn on the power supply, the device runs, and the separation process Keep the temperature of the feed liquid at 30-35°C, the operating pressure is 1.6-2.0MP, and the feed liquid is circulated on the upstream side of the membrane, and the primary permeate is collected downstream. When the collection volume of the primary permeate is 7L, the equipment is closed; Add 7.5L of the mixed solution of vegetable oi...
Embodiment 2
[0042] The present embodiment relates to the removal of hazardous components in capsanthin. Compared with Example 1, the difference lies in the different consumption of organic solvents, including the following steps:
[0043] Dissolve 1000g of capsanthin (color value 145.2, benzopyrene 26ppb, total Sudan red (Sudan red I-IV) 200ppb, rhodamine B65ppb, ethion 36ppm, chlorpyrifos 12ppm, triazophos 21ppm) into vegetable oil for extraction. The mixed solution of solvent and acetone (vegetable oil extraction solvent: acetone=3:2) 20000ml, filtered to remove solid insolubles, put the feed liquid into the feed tank of the organic solvent-resistant nanofiltration membrane equipment, turn on the power supply, the device is running, during the separation process Keep the temperature of the feed liquid at 30-35°C, and the operating pressure at 1.6-2.0MPa. The feed liquid is circulated on the upstream side of the membrane, and the permeate is collected downstream. When the collection volum...
Embodiment 3
[0046] Compared with Example 1, the difference is that the organic solvent is ethyl acetate.
[0047] The present embodiment relates to the removal of harmful components in capsanthin, including the following steps:
[0048] 1) Dissolve 1000 g of capsanthin (color value 145.2, benzopyrene 26 ppb, total Sudan red (Sudan red I-IV) 200 ppb, rhodamine B 65 ppb, ethion 36 ppm, chlorpyrifos 12 ppm, triazophos 21 ppm) into acetic acid. 10000ml of ethyl ester, filtered to remove solid insolubles, put the feed liquid into the feed liquid tank of the organic solvent-resistant nanofiltration membrane equipment, turn on the power supply, and run the device. During the separation process, keep the feed liquid temperature at 30-35 ℃, and the operating pressure is 1.6-2.0 MPa. The feed liquid is circulated on the upstream side of the membrane, the primary permeate is collected downstream, and the equipment is closed when the collection volume of the primary permeate is 7L; 7.5L of ethyl ace...
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