A kind of graphene radiation heating film and preparation method thereof
A graphene and heating film technology, applied in the field of material engineering, can solve the problem of high cost and achieve the effects of low cost, stable performance and high thermal power
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Embodiment 1
[0044] A kind of preparation method of graphene radiation heating film:
[0045] First prepare the heating layer spray liquid, the method is as follows:
[0046] Step 1: Take 20Kg of crystalline tin tetrachloride, pour it into a plastic barrel with a volume of more than 100 liters, then add 50Kg of industrial alcohol with a concentration of 75% by volume and soak for 24 hours, stir with a plastic rod occasionally, let the four Tin chloride is completely soluble in alcohol.
[0047] The second step: Take 21 grams of graphene and pour it into the solution prepared in the first step.
[0048] The third step: take 200 grams of ferric chloride and put it into a glass vessel with a volume of 2 liters, add 1000 milliliters of industrial alcohol with a concentration of 75%, heat it with a heating device, and stir it magnetically. After it is completely dissolved, put Pour all the dissolving solution into the solution prepared in the first step and the second step, mix and stir evenl...
Embodiment 2
[0052] A kind of preparation method of graphene radiation heating film:
[0053] Graphene oxide is prepared first.
[0054]The preparation method of described graphene oxide is, take 1g graphene powder, 0.5g sodium nitrate, 1g potassium permanganate and add in the flask of ice-water bath, add 20ml concentrated sulfuric acid by dropwise, stir slowly, after adding 10ml Add 1g of potassium permanganate when concentrated sulfuric acid is added, and then add 1g of potassium permanganate after adding 20ml of concentrated sulfuric acid, then slowly stir until the liquid is slightly yellow, heat up to 80°C, then add 50ml of deionized water dropwise, and react for 1h . Then add 100ml of deionized water, and then dropwise add 30% hydrogen peroxide until the liquid is bright yellow. After filtering, wash with 10% dilute hydrochloric acid until no sulfate ion is detected, and then wash with deionized water until the pH of the washing solution is stable. Soak in 0.01% (v / v) Tween 80 dei...
Embodiment 3
[0058] A kind of preparation method of graphene radiation heating film:
[0059] The difference from Example 2 is that in the method for preparing the heat-generating layer spray liquid, the amount of graphene oxide used is 0.8 g. The remaining parameters include the amount of mixed liquid consumed, the carrier and the area sprayed on the carrier, and the time is the same.
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