High-temperature oxidation resistant low-viscosity synthetic ester as well as preparation method and application thereof
A high-temperature oxidation-resistant and ester-synthesizing technology, used in lubricating compositions, base materials, petroleum industry, etc., can solve problems such as being unsuitable for air compressor oil and heat-conducting oil systems, the inability of degradants to be effectively dispersed, and high-temperature oxidation.
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Embodiment 1
[0027] The high-temperature oxidation-resistant low-viscosity synthetic ester described in this embodiment, the raw materials for its preparation include the following components:
[0028] Trimethylolpropane 15mol;
[0029] Neopentyl glycol 10mol;
[0030] Succinic acid 12mol;
[0031] 1,4-cyclohexanedicarboxylic acid 4mol;
[0032] 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionic acid 4mol;
[0033] Triethylchlorosilane 15mol;
[0034] Tripropylchlorosilane 32mol;
[0035] Xylene 20mol;
[0036] Monobutyltin oxide 0.02mol;
[0037] Anhydrous sodium carbonate 16.5mol.
[0038] The preparation method of the high-temperature oxidation-resistant low-viscosity synthetic ester described in this embodiment comprises the following steps:
[0039] (1) Take the described trimethylolpropane, neopentyl glycol, succinic acid, 1,4-cyclohexanedicarboxylic acid, 3-(3,5-di-tert-butyl-4-hydroxy Phenyl)propionic acid, monobutyl tin oxide catalyst, and xylene are added to the reaction ket...
Embodiment 2
[0044] The high-temperature oxidation-resistant low-viscosity synthetic ester described in this embodiment, the raw materials for its preparation include the following components:
[0045] Trimethylolpropane 25mol;
[0046] Neopentyl glycol 5mol;
[0047] Succinic acid 9mol;
[0048] 1,4-cyclohexanedicarboxylic acid 6mol;
[0049] 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionic acid 6mol;
[0050] Triethylchlorosilane 25mol;
[0051] Tripropylchlorosilane 44mol;
[0052] Xylene 30mol;
[0053] Monobutyltin oxide 0.06mol;
[0054] Anhydrous sodium carbonate 25mol.
[0055] The preparation method of the high-temperature oxidation-resistant low-viscosity synthetic ester described in this embodiment comprises the following steps:
[0056] (1) Take the described trimethylolpropane, neopentyl glycol, succinic acid, 1,4-cyclohexanedicarboxylic acid, 3-(3,5-di-tert-butyl-4-hydroxy Phenyl)propionic acid, monobutyl tin oxide catalyst, and xylene are added to the reaction kettle, m...
Embodiment 3
[0061] The high-temperature oxidation-resistant low-viscosity synthetic ester described in this embodiment, the raw materials for its preparation include the following components:
[0062] Trimethylolpropane 20mol;
[0063] Neopentyl glycol 8mol;
[0064] Succinic acid 7mol;
[0065] 1,4-cyclohexanedicarboxylic acid 8mol;
[0066] 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionic acid 3mol;
[0067] Triethylchlorosilane 22mol;
[0068] Tripropylchlorosilane 39mol;
[0069] Xylene 25mol;
[0070] Monobutyltin oxide 0.06mol;
[0071] Anhydrous sodium carbonate 22mol.
[0072] The preparation method of the high-temperature oxidation-resistant low-viscosity synthetic ester described in this embodiment comprises the following steps:
[0073] (1) Take the described trimethylolpropane, neopentyl glycol, succinic acid, 1,4-cyclohexanedicarboxylic acid, 3-(3,5-di-tert-butyl-4-hydroxy Phenyl)propionic acid, monobutyl tin oxide catalyst, and xylene are added to the reaction kettle,...
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