A method for detecting trace rare earth elements
A rare earth element and trace technology, applied in the field of rare earth element detection, can solve the problem that the determination of trace rare earth elements is not ideal, and achieve the effect of improving sensitivity and accurate determination
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Embodiment 1
[0051] The present embodiment adopts the external standard method (working curve method) combined with the internal standard correction method. At low resolution R=300 for 45 Sc, 89 Y, 139 La, 140 Ce, 141 Pr, 146 Nd, 147 Sm, 153 Eu, 158 Gd, 159 Tb, 163 Dy, 166 Two, 169 Tm, 172 Yb and 175 Lu was measured.
[0052] For mixed standard element solutions with working curve concentrations of 0.00, 0.10, 0.50, 1.00, and 5.00ng / ml, the signal of the target element has a linear relationship with the concentration, and the correlation coefficient of the linear equation has reached the level of 0.9999, which is conducive to the accurate determination of traces in geological samples concentration of rare earth elements. The concentration of the mixed standard solution is diluted to 10 μg / ml, using 2% (V / V) HNO 3 Diluted step by step, and added 1ng / ml In as internal standard to the working curve mixed standard solution.
[0053] Step 1 Sample Digestion
[0054] Six nation...
Embodiment 2
[0067] The detection method is the same as in Example 1 except that the nitrogen flow rate is limited to 0 mL / min.
Embodiment 3
[0069] The detection method is the same as in Example 1 except that the nitrogen flow is limited to 3mL / min.
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