Long-acting rice pre-emergence special herbicide and preparation method thereof
A herbicide and rice seedling technology, applied in the direction of herbicides and algicides, botanical equipment and methods, plant growth regulators, etc., can solve the problem of affecting the emergence and growth of rice seedlings, poor weed control effect, and drug efficacy Low stability and other problems, to achieve a good effect of sealing grass, maintain the number of emergence and growth quality, maintain the effect of emergence rate and growth quality
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Embodiment 1
[0031] Embodiment 1-a kind of preparation method of long-acting rice pre-emergence special herbicide, comprises the steps:
[0032] (1) mixing urea and a 37% formaldehyde solution with a mass concentration of 1:2 in a molar ratio, and heating and mixing in a 70° C. water bath for 2h, with a pH value of 8.0, to obtain a urea-formaldehyde prepolymerization solution;
[0033] (2) using bensulfuron-methyl, bispyribac, clomazone and acetone, carry out ultrasonic stirring and mixing according to the weight ratio of 0.2:0.8:2:14 to obtain the initial mixed solution of herbicide A; Acetochlor and acetone are 1:1:16 to carry out ultrasonic stirring and mixing according to the weight ratio to obtain the initial mixed solution of herbicide B;
[0034] Wherein, the frequency of ultrasonic mixing is 30kHz, the power of ultrasonic treatment is 300W, the time of ultrasonic treatment is 5min, and the stirring speed is 200r / min;
[0035] (3) Mix the initial mixed solution of herbicide A, chit...
Embodiment 2
[0041] Embodiment 2-a kind of preparation method of long-acting rice pre-emergence special herbicide, comprises the steps:
[0042] (1) mixing urea with a 37% formaldehyde solution in a molar ratio of 1:2, and heating and mixing in a water bath at 80°C for 2.5h, with a pH value of 8.0, to obtain a urea-formaldehyde prepolymerization solution;
[0043](2) using bensulfuron-methyl, bispyribac, clomazone and acetone, carry out ultrasonic stirring and mixing according to the weight ratio of 0.5:1.2:3:18 to obtain the initial mixed solution of herbicide A; Acetochlor and acetone are carried out ultrasonic stirring and mixing according to the weight ratio of 3:3:28 to obtain the initial mixed solution of herbicide B;
[0044] Among them, the frequency of ultrasonic mixing is 35kHz, the power of ultrasonic treatment is 400W, the time of ultrasonic treatment is 10min, and the stirring speed is 400r / min;
[0045] (3) Mix the initial mixed solution of herbicide A, chitosan, dispersant,...
Embodiment 3
[0051] Embodiment 3-a kind of preparation method of long-acting rice pre-emergence special herbicide, comprises the steps:
[0052] (1) mixing urea and a 37% formaldehyde solution with a mass concentration of 1:2 in a molar ratio, and heating and mixing in a 75°C water bath for 2.0h, with a pH value of 8.0, to obtain a urea-formaldehyde prepolymerization solution;
[0053] (2) using bensulfuron-methyl, bispyribac, clomazone and acetone, carry out ultrasonic stirring and mixing according to the weight ratio of 0.3:1.0:2.5:16 to obtain the initial mixed solution of herbicide A; Acetochlor and acetone are ultrasonically stirred and mixed according to the weight ratio of 2:2:20 to obtain the initial mixed solution of herbicide B;
[0054] Among them, the frequency of ultrasonic mixing is 35kHz, the power of ultrasonic treatment is 350W, the time of ultrasonic treatment is 8min, and the stirring speed is 300r / min;
[0055] (3) Mix the initial mixed solution of herbicide A, chitosa...
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