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Novel rare earth nano-composite cleaning antibacterial antifogging agent as well as preparation method and application thereof

A nano-composite, anti-fogging agent technology, applied in chemical instruments and methods, other chemical processes, paints containing biocides, etc. To achieve the effect of enhanced hydrophilicity, good dispersion and adhesion, and prolonged anti-fog time

Pending Publication Date: 2020-11-03
TIANJIN BAOGANG RES INST OF RARE EARTHS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In recent years, with the development of society, transparent substrates such as glass and resin have become indispensable materials in daily life and industrial production, and are widely used in mirrors, lenses, automotive glass, etc. However, when there is a temperature difference between its two sides, when the saturated vapor pressure of moisture on the lower surface is lower than the vapor pressure of the surrounding environment, the water vapor will accumulate on the surface of the object and precipitate into fog in the form of tiny water droplets, thereby affecting vision Effects such as fogging of glasses in winter, fogging of glasses caused by breathing after wearing a mask, fogging of nurses' goggles in the fight against the epidemic, fogging of car windows, etc., have caused a lot of inconvenience and affected safety.
[0003] The current anti-fogging agent products have problems such as short anti-fogging time, easy to wipe off the anti-fogging film when exposed to water or inadvertent scratches, and high cost. , cleaning and antibacterial effects are also extremely important, and the current defogger products lack these functions

Method used

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  • Novel rare earth nano-composite cleaning antibacterial antifogging agent as well as preparation method and application thereof
  • Novel rare earth nano-composite cleaning antibacterial antifogging agent as well as preparation method and application thereof
  • Novel rare earth nano-composite cleaning antibacterial antifogging agent as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Nanoscale rare earth oxides were synthesized by sol-gel method, and the TEM scanning electron microscope images of nanoscale rare earth oxides are shown in figure 1 Synthesize rare earth-loaded nano-titanium dioxide by impregnation method, mix the two in proportion, and disperse evenly in the aqueous solution by ultrasonication for 5 minutes to obtain a nano-rare-earth oxide composite dispersion, and disperse the prepared nano-rare-earth oxide composite dispersion in a diluent Deionized water, then add solvent, surfactant, lubricant, chelating agent, mix and stir evenly to obtain a new type of rare earth nano-composite cleaning antibacterial antifogging agent. Wherein, the parts by weight of each component are as follows:

[0044]

[0045]

[0046] Wherein: the solvent is a mixed solution of ethanol and isopropanol in a weight ratio of 3:1; the weight ratio of alcohol ether glycoside AEG-10 and fluorocarbon surfactant is 9:1; the nano-rare earth oxide is nano-ceri...

Embodiment 2

[0075] Nano-scale rare earth oxides were synthesized by precipitation method, rare earth-loaded nano-titanium dioxide was synthesized by impregnation method, the two were mixed in proportion, and ultrasonically dispersed in aqueous solution for 40 minutes to obtain a composite dispersion of nano-rare earth oxides, and the prepared nano-rare earth The oxide composite dispersion liquid is dispersed in the diluent deionized water, then a solvent, a surfactant, a lubricant, and a chelating agent are added, and after mixing, the mixture is evenly stirred to obtain a new type of rare earth nano-composite cleaning, antibacterial and antifogging agent. Wherein, the parts by weight of each component are as follows:

[0076]

[0077]

[0078] Among them: the solvent is a mixed solution of ethanol and isopropanol in a weight ratio of 1:1; the weight ratio of cetyltrimethylammonium bromide and polyvinylpyrrolidone is 7:3; Lanthanum; rare earth-loaded nano-titanium dioxide is cerium-...

Embodiment 3

[0081] Nanoscale rare earth oxides were synthesized by hydrothermal method, rare earth loaded nano titanium dioxide was synthesized by impregnation method, the two were mixed in proportion, and ultrasonically dispersed in aqueous solution for 60 minutes to obtain nano rare earth oxide composite dispersion liquid, and the prepared nano The rare earth oxide composite dispersion liquid is dispersed in the diluent deionized water, then a solvent, a surfactant, a lubricant, and a chelating agent are added, and after mixing, the mixture is evenly stirred to obtain a new type of rare earth nanocomposite cleaning antibacterial and antifogging agent. Wherein, the parts by weight of each component are as follows:

[0082]

[0083]

[0084] Among them: the solvent is a mixture of ethanol and isopropanol in a weight ratio of 2:1; the weight ratio of polyvinyl alcohol and fluorocarbon surfactant is 5:2; the nano-rare earth oxide is nano-praseodymium oxide; the rare-earth-loaded nano-t...

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PUM

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Abstract

The invention provides a novel rare earth nano composite cleaning antibacterial antifogging agent and a preparation method and application thereof. The novel rare earth nano composite cleaning antibacterial antifogging agent is prepared from, by weight, 0.2-30% of nano rare earth oxide composite dispersion liquid, 0.05-6% of surfactant, 10-25% of solvent, 0.2-5% of lubricant and 0.05-2% of chelating agent, and the balance is a diluent; wherein the nano rare earth oxide composite dispersion liquid is a composite dispersion liquid of nano rare earth oxide and rare earth supported nano titanium dioxide. The novel rare earth nano-composite cleaning antibacterial antifogging agent is remarkable in demisting effect, stable in performance, low in cost, green and non-toxic, and has cleaning and antibacterial functions.

Description

technical field [0001] The invention belongs to the field of antifogging agent preparation, and in particular relates to a novel rare earth nano-composite cleaning antibacterial antifogging agent and its preparation method and application. Background technique [0002] In recent years, with the development of society, transparent substrates such as glass and resin have become indispensable materials in daily life and industrial production, and are widely used in mirrors, lenses, automotive glass, etc. However, when there is a temperature difference between its two sides, when the saturated vapor pressure of moisture on the lower surface is lower than the vapor pressure of the surrounding environment, the water vapor will accumulate on the surface of the object and precipitate into fog in the form of tiny water droplets, thereby affecting vision Effects, such as fogging of glasses in winter, fogging of glasses caused by breathing after wearing a mask, fogging of nurses' goggl...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D1/00C09D5/14C09K3/18G02C7/02G02B1/18
CPCC09D1/00C09D5/14C09K3/18G02C7/02G02B1/18
Inventor 李璐秦晓婷温永清赵长玉尹健邓冠南
Owner TIANJIN BAOGANG RES INST OF RARE EARTHS
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