School uniform manufacturing technology based on heat-storage polyacrylonitrile warmth-keeping fiber fabric
A technology of polyacrylonitrile fiber and manufacturing process, which is applied in the direction of fiber type, fiber treatment, plant fiber, etc.
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Embodiment 1
[0027] The raw materials of the surface layer of the school uniform in this embodiment are cotton fiber and polyacrylonitrile fiber; the raw materials of the inner layer are hemp fiber and viscose fiber; wherein, the mass ratio of cotton fiber to polyacrylonitrile in the raw material of the surface layer is 6:1; The mass ratio of fiber and viscose fiber is 8:1.
[0028] Step 1: Add trimesoyl chloride to 30# paraffin at 40°C and mix evenly. The mass ratio of trimesoyl chloride and 30# paraffin is 1:10 to obtain mixture I; Min emulsified for 5 seconds to obtain an emulsion. Take ethylenediamine with a mass equal to 1% of the water phase emulsion, add dropwise to dissolve and emulsify, react at a constant temperature of 40°C for 30 minutes, and dry in vacuum to obtain microcapsules.
[0029] Step 2, polyacrylonitrile is dissolved in the sodium thiocyanate solution of 51wt%, obtains solution II, then microcapsule is added in the solution II, makes spinning solution; Polyacrylonitr...
Embodiment 2
[0042] The material of the surface layer of the school uniform in this embodiment is cotton fiber and polyacrylonitrile fiber; the material of the inner layer is hemp fiber and viscose fiber; wherein, the mass ratio of cotton fiber to polyacrylonitrile in the material of the surface layer is 7:1; The mass ratio of fiber and viscose fiber is 9:1.
[0043]Step 1: Add trimesoyl chloride to 30# paraffin at 40°C and mix evenly. The mass ratio of trimesoyl chloride and 30# paraffin is 1:10 to obtain mixture I; Min emulsified for 5 seconds to obtain an emulsion. Take ethylenediamine with a mass equal to 1% of the water phase emulsion, add dropwise to dissolve and emulsify, react at a constant temperature of 40°C for 30 minutes, and dry in vacuum to obtain microcapsules.
[0044] Step 2, polyacrylonitrile is dissolved in the sodium thiocyanate solution of 51wt%, obtains solution II, then microcapsule is added in the solution II, makes spinning solution; Polyacrylonitrile polymer and m...
Embodiment 3
[0058] The material of the surface layer of the school uniform in this embodiment is cotton fiber and polyacrylonitrile fiber; the material of the inner layer is hemp fiber and viscose fiber; wherein, the mass ratio of cotton fiber to polyacrylonitrile in the material of the surface layer is 7:1; The mass ratio of fiber and viscose fiber is 8:1. Preparation method is identical with embodiment 1 or 2.
[0059] The modified polyacrylonitrile fiber physical properties prepared by the present embodiment are as follows:
[0060] Table 3: Modified polyacrylonitrile fiber physical properties prepared by embodiment 3
[0061]
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