A fixed bed flow reactor and its application

A reactor and fixed bed technology, applied in the field of up-flow reactors, can solve problems such as adverse effects on the reaction process, blockage of the distributor, and impact on fluid distribution, etc., so as to achieve a uniform catalyst bed pressure drop, and a reduction in the amount of dust generated and reduced. The effect of local resistance

Active Publication Date: 2021-10-08
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Since the catalyst particles cannot pass through the small bed support gap, these particles are likely to block the distributor or bed support, resulting in uneven distribution of fluid, especially gas, which affects the distribution of fluid in the reactor and affects the reaction process. adversely affect
At the same time, it will also be accompanied by the wear and pulverization of the catalyst particles, resulting in a large amount of catalyst dust. These dusts move upward with the reaction materials, and clogging occurs on the surface of the screen or grid, resulting in a rapid increase in the pressure drop of the bed, affecting response start cycle

Method used

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  • A fixed bed flow reactor and its application
  • A fixed bed flow reactor and its application
  • A fixed bed flow reactor and its application

Examples

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Effect test

Embodiment 1

[0051] Using the upflow reactor of the present invention, the raw oil and hydrogen are mixed with a conventional static mixer (model SV2.3 / 25-6.4-500), and then the mixture is introduced into the upflow as the reactor feed The reactor (reactor diameter is 100mm), along the material flow direction in the reactor are the lower sliding grid 80mm, the first catalyst bed 400mm, the linkage filter dust layer 260mm, the second catalyst bed 800mm, the upper sliding grid The grid is 60mm; the lower sliding grid includes the slideway and the grid plate, and the length of the slideway is 80mm; the upper sliding grid includes the slideway and the grid plate, and the length of the upper slideway is 60mm; the linkage filter dust layer includes the upper linkage layer , filter dust layer, lower linkage layer; upper linkage layer includes upper slideway group, upper linkage layer first fixing plate, upper linkage layer second fixing plate, lower linkage layer includes glide path group, lower l...

Embodiment 2

[0053] Using the up-flow reactor of the present invention, the raw oil and hydrogen are mixed with an inorganic membrane tube disperser. First, the hydrogen is dispersed into microbubbles with a size of 50 nm and then penetrates out of the tube to form a reaction with the liquid introduced into the shell. The mixture is fed into the reactor, and then the mixture is introduced into the up-flow reactor as the reactor feed (reactor diameter is 200 mm). The grid is 100mm, the first catalyst bed is 800mm, the linkage filter dust layer is 300mm, the second catalyst bed is 600mm, the upper sliding grid is 80mm, and the gland is 100mm; The upper surface of the grid is tiled with 10-mesh stainless steel; the lower sliding grid includes slideways and grid plates, and the length of the lower slides is 100mm; the upper sliding grid includes slides and grid plates, and the length of the upper slides is 80mm; linkage The filter dust layer includes an upper linkage layer, a filter dust layer...

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Abstract

The invention discloses a fixed-bed flow-type reactor. The reactor includes a reactor shell, in which a lower sliding grid, a first catalyst bed, a linkage filter dust accumulation layer, and a material flow direction are arranged in the reactor shell. The second catalyst bed layer and the upper sliding grid; the filter dust layer is fixedly connected with the upper sliding grid and the lower sliding grid respectively through support rods, and the reaction material inlet is arranged at the bottom of the reactor shell, and the reactor shell The top is provided with a reaction material outlet. The reactor is equipped with a linkage filter dust layer, which can effectively reduce the movement wear between the catalyst particles, improve the service life of the catalyst, continuously remove the catalyst dust during the reaction process, improve the uniformity of the reaction, and greatly slow down the catalyst bed. The layer pressure drop increases to maintain the long-term stable operation of the reactor.

Description

technical field [0001] The invention belongs to the field of petrochemical equipment, and relates to an up-flow reactor and its application. Background technique [0002] In the field of petrochemical industry, hydrogenation process is an important technical means to treat distillate oil and secondary processed oil. Through hydrogenation, impurities such as sulfur, nitrogen, metal, colloid and carbon residue in oil products can be effectively removed. Removal and hydroconversion of unsaturated hydrocarbons to saturated hydrocarbons. According to the type of reactor, hydrogenation process can be divided into fixed bed hydrogenation process, suspended bed hydrogenation process and ebullated bed hydrogenation process, among which the fixed bed hydrogenation process is the most widely used. [0003] According to the feeding method of the fixed-bed reactor, it can be divided into two types: up-flow or down-feed and down-flow or up-feed fixed-bed reactor. The up-flow fixed-bed re...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/04C10G49/00
CPCB01J8/0446B01J8/0492B01J2208/00884C10G49/00C10G2300/4006C10G2300/4012
Inventor 周嘉文杨秀娜阮宗琳王昊晨姜阳崔国英关明华
Owner CHINA PETROLEUM & CHEM CORP
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