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A preparation method for intermediate transition layer applied in vacuum diffusion welding

A technology of vacuum diffusion and transition layer, applied in welding equipment, vacuum evaporation coating, coating, etc., can solve the problems of poor welding quality of structural parts, difficulty in achieving close and uniform fit of nickel foil and welding surface, low purity, etc. , to achieve the effect of improving welding quality, easy to fit tightly and evenly, and high purity

Active Publication Date: 2022-03-01
AVIC LIYUAN HYDRAULIC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The electroplating film method and the chemical plating film method are prepared by chemical methods. The film layer prepared as the intermediate transition layer inevitably contains metal impurities, the purity is low, and the thickness is thin. The quality of the intermediate transition layer is poor. To a certain extent The welding quality of structural parts will be poor; the pure nickel foil method can be used for diffusion welding between planes, but for parts whose welding surface is a deep curved surface, it is difficult to achieve a close and uniform fit between the nickel foil and the welding surface, and the intermediate transition layer The poor quality of the structure will also make the welding quality of the structural parts poor
[0003] Therefore, the intermediate transition layer prepared by the existing preparation method has the defect of containing metal impurities, which will make the welding quality of the structural parts poor; or has the defect that it is difficult to closely and evenly fit the welding surface of the deep curved surface, which will also make the welding quality of the structural parts poor.

Method used

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  • A preparation method for intermediate transition layer applied in vacuum diffusion welding
  • A preparation method for intermediate transition layer applied in vacuum diffusion welding

Examples

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Embodiment 1

[0033] Example 1. A method for preparing an intermediate transition layer applied to vacuum diffusion welding. A nickel film is prepared on the welding surface of a part (made of tin bronze, material grade QSn6.5-0.1), comprising the following steps,

[0034] Preliminary preparation work, prepare the nickel target, the purity of the nickel target is 99.99%, and the thickness is 4mm, put the nickel target into the sputtering chamber of the magnetron sputtering coating equipment, connect the nickel target to the DC power supply in the sputtering chamber, adjust The distance between the nickel target and the workpiece holder is between 100-180mm.

[0035] a. Soak the parts in gasoline for 20, 25 or 30 minutes, preferably 25 minutes, to obtain product A;

[0036] b. Wash product A with tap water for 1, 2 or 3 minutes, preferably 2 minutes, to obtain product B;

[0037] c. Use 15%, 18% or 20% concentration of HNO 3 Pickling product B with solution for 1, 1.5 or 2 minutes, the op...

Embodiment 2

[0048] Example 2. A method for preparing an intermediate transition layer applied to vacuum diffusion welding. Compared with Example 1, the only difference is that the material of the part is tin bronze, the brand name is ZQSn10-2-3.

Embodiment 3

[0049] Example 3. A method for preparing an intermediate transition layer applied to vacuum diffusion welding. Compared with Example 1, the only difference is that the material of the part is alloy steel, brand 40CrNiMoA.

[0050] The finished product gained in embodiment 1 and the finished product gained in embodiment 3 are carried out vacuum diffusion welding, from figure 1 It can be seen that the intermediate transition layer (that is, the coating or nickel layer) has a very good diffusion connection effect. After measurement, the thickness of the transition layer (the transition layer is composed of the intermediate transition layer plated on the two finished products) reaches 20um. The thickness is uniform, the tensile strength between the two finished products is ≥320 MPa, and the welding quality is good.

[0051] The finished product gained in embodiment 2 and the finished product gained in embodiment 3 are carried out vacuum diffusion welding, from figure 2 It can b...

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Abstract

The invention discloses a preparation method for an intermediate transition layer applied in vacuum diffusion welding, which is characterized in that it comprises the following steps: a. soaking parts in gasoline to obtain product A; b. cleaning product A to obtain product B; c. Use HNO 3 Pickling product B with solution to obtain product C, d, cleaning product C, obtaining product D, e, washing product D with HCl solution, obtaining product E, f, cleaning product E, obtaining product F, g, cleaning product F with alcohol, Get product G, h, dry product G, get product H, i, preheat product H in a vacuum environment, get product I, j, clean product I with Hall source, get product J, k, ion bombard product J , so that the J product is activated to obtain the K product, the l and K products are pre-coated to obtain the L product, and the m and L products are coated to obtain the finished product. The intermediate transition layer prepared by the invention has the advantage of high purity, which can make the welding quality of the structural parts good; it also has the advantage of being easy to fit closely and evenly with the welding surface of the deep curved surface, and can also make the welding quality of the structural parts good.

Description

technical field [0001] The invention belongs to the field of vacuum welding diffusion welding, and in particular relates to a preparation method for an intermediate transition layer applied in vacuum diffusion welding. Background technique [0002] In modern engineering applications, the performance requirements of structural parts are getting higher and higher. In order to meet the performance requirements of structural parts, it is often necessary to connect two parts of different materials and performance differences, such as two parts of different metal materials. , or metal parts and ceramic parts are connected together, however, it is difficult to achieve the above connection using traditional fusion welding, vacuum diffusion welding, one of the special welding methods, is an effective way for the above connection. Before vacuum diffusion welding, it is necessary to prepare an intermediate transition layer on the welding surface of the parts, and the quality of the int...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/34C23G1/02C23G5/00
CPCB23K1/20C23G1/02C23G5/032C23G5/00C23C14/34
Inventor 林钰唐江滕海山陈杰吴小芳杨先石登明
Owner AVIC LIYUAN HYDRAULIC
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