Regular carrier catalyst with desulfurization effect as well as preparation and application thereof
A technology for regular carrier and desulfurization, which is applied to a regular carrier catalyst with desulfurization and its preparation and application fields, can solve the problems of loss of octane number, decrease of desulfurization activity, decrease of octane number of gasoline products, etc.
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preparation example Construction
[0055] The method for preparing a structured carrier catalyst provided by the invention includes the step of preparing a suspension. The preparation method of the suspension includes: forming a mixture of metal powder, a hydroxyl-containing solvent and a surfactant, and treating it under ultrasonic waves to obtain a mixed liquid after ultrasonic treatment; wherein, during the ultrasonic treatment process, the fine particles are peeled off from the metal powder The metal particles are suspended in a hydroxyl-containing solvent (solvent for short); the larger particles are separated from the ultrasonically mixed solution to obtain a suspension, and the suspension contains fine particles containing modified metals. The metal powder (also known as metal powder) can be pure metal powder (when the metal film only contains modified metal and the modified metal is one kind), alloy powder containing modified metal and boron, containing Alloy powder of various modified metals. Among th...
Embodiment approach
[0069] According to the first embodiment described in the method for preparing a structured carrier catalyst of the present invention, preferably, the weight of the source of alumina calculated as alumina and the source of oxides of at least one metal in Group IIA and Group IIB calculated as oxides The ratio is 0-80:20-100, for example, 0-70:30-100 or 0-60:40-100 or 0-50:50-100 or 25-60:40-75 or 60-70:30-40.
[0070] According to the preparation method of the structured carrier catalyst of the present invention, the coating is such that in the product obtained by coating, the content of the active coating is 10 to 50% by weight, preferably 15 to 30% by weight, on a dry basis, More preferably 20-30% by weight. The coating is carried out one or more times. Preferably, drying and optional firing are carried out after each coating, and firing is carried out after the last coating, so that the content of the active coating in the obtained product meets the requirements.
[0071] A...
specific Embodiment approach
[0078] A specific embodiment of the preparation method of the structured carrier catalyst provided by the present invention includes the following steps: uniformly mixing the metal powder and the hydroxyl-containing solvent, and then using a specific ultrasonic power of 50-250W / (100g hydroxyl-containing solvent), preferably 100- Ultrasonic treatment at a power of 150W / (100g hydroxyl-containing solvent) for 4 to 10 hours, for example, 5 to 8 hours, and then centrifuge the ultrasonically mixed solution at 1200 to 3000 rpm, preferably 1500 to 2500 rpm, to obtain Suspension liquid; then mix matrix particles with the suspension liquid, disperse evenly, freeze-dry, and coat the regular carrier to prepare the regular carrier catalyst. The average particle size of the metal powder is less than 20 microns, preferably 1-15 microns or 3-18 microns; the metal powder: hydroxyl-containing solvent = 1:2-15 weight ratio, preferably 1:5-10; Said surfactant: solvent=0.001~100mg:1mL is for examp...
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