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Natural antibacterial moisturizing mask preparation method

A natural antibacterial and nanofiber membrane technology, which is applied in skin care preparations, pharmaceutical formulations, cosmetic preparations, etc., can solve the problems of tightness, reduced mask use effect, and discomfort, so as to increase the abundance, The effect of improving bioavailability

Active Publication Date: 2020-01-03
广州黛香源生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, the beauty and skin care masks on the market are basically made of chemical synthetic fiber non-woven fabrics or artificial fiber non-woven fabrics through processes such as folding, bagging, injecting soaking liquid, and sealing, but synthetic fiber non-woven fabrics or artificial fiber Non-woven fabrics generally have degradation problems, and they cannot be recycled, and they are easy to cause environmental pollution after consumers use them.
The fibers and adhesives of non-woven fabrics will partially dissolve under long-term immersion in soaking liquid, thus reducing the use effect of the mask and even causing allergies to consumers
In addition, the soaking solution of commonly used facial masks is thickened with polymer synthetic resin, consumers will feel tight after use and feel uncomfortable when using it

Method used

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  • Natural antibacterial moisturizing mask preparation method
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preparation example Construction

[0028] A preparation method of a natural antibacterial water-retaining facial mask, comprising the steps of:

[0029] S1: dissolving polyglutamic acid and polylysine in a trifluoroacetic acid solution, stirring evenly to obtain a spinning solution;

[0030] S2: using the spinning solution to perform electrospinning to obtain a PGA / PL nanofiber membrane;

[0031] S3: activating the PGA / PL nanofiber membrane by plasma treatment to obtain an activated nanofiber membrane;

[0032] S4: Soak the nanofibrous membrane obtained in step S3 in octacosanol lipase solution for negative pressure flash explosion, after esterification and grafting reaction, centrifuge and freeze-dry to obtain a natural antibacterial and water-retaining mask.

[0033] Firstly, dissolving polyglutamic acid and polylysine in trifluoroacetic acid solution and stirring evenly to obtain spinning solution. The sources of polyglutamic acid and polylysine are not limited in the present invention, and commercially av...

Embodiment 1

[0039] S1. Weigh 1.5g of polyglutamic acid with an average molecular weight of 600kDa and 0.6g of polylysine with an average molecular weight of 3500Da and completely dissolve them in 100ml of 5% (v / v) trifluoroacetic acid solution, stir evenly to obtain a spinning solution;

[0040]S2. Electrospinning is carried out with the spinning liquid, the syringe used is 10ml, the needle is flat, No. 7 needle; the electrospinning conditions are: voltage 18KV, distance 9cm, injection rate 0.5ml / h, temperature 30°C Obtain PGA / PL nanofiber film;

[0041] S3, the PGA / PL nanofiber membrane is activated by plasma processor treatment, the conditions of plasma treatment are: the gas adopts oxygen, the treatment power is 280W, the pressure is 55Pa, and the treatment time is 12min;

[0042] S4, soak the nanofibrous film obtained in step S3 in the ethanol solution of octacosanol lipase containing 6g / L octacosanol, 40g / L activity is 50U / mg lipase and carry out negative pressure flash explosion, ne...

Embodiment 2

[0045] S1. Weigh 0.5g of polyglutamic acid with an average molecular weight of 200kDa and 0.4g of polylysine with an average molecular weight of 3000Da and completely dissolve them in 100ml of 5% (v / v) trifluoroacetic acid solution, stir evenly to obtain a spinning solution;

[0046] S2. Electrospinning is carried out with the spinning liquid, the syringe used is 10ml, the needle is flat, and the needle is No. 7; the electrospinning conditions are: voltage 12KV, distance 7cm, injection rate 0.3ml / h, temperature 25°C Obtain PGA / PL nanofiber film;

[0047] S3, the PGA / PL nanofiber membrane is activated by a plasma processor, and the conditions of the plasma treatment are: the gas is nitrogen, the processing power is 250W, the pressure is 50Pa, and the processing time is 10min;

[0048] S4, soak the nanofibrous film that step S3 obtains in containing 4g / L octacosanol, 20g / L activity is the octacosanol lipase ethanol solution of 30U / mg lipase and carry out negative pressure flash ...

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Abstract

The invention discloses a natural antibacterial moisturizing mask preparation method. The method includes: (1) completely dissolving a certain quantity of polyglutamic acid and polylysine into 5v / v% trifluoroacetic acid solution, and well stirring to obtain spinning solution; (2) performing electrostatic spinning by the spinning solution to obtain a PGA / PL nanofiber membrane; (3) subjecting the PGA / PL nanofiber membrane to treatment and activation through a plasma processor; (4) soaking activated nanofibers in octacosanol lipase solution to realize negative-pressure flash explosion, then performing esterification grafting reaction, and carrying out centrifugal freeze drying. A mask prepared according to the method is environmentally friendly and degradable, has efficient moisture absorbing, moisturizing and activating effects on the skin and can be applied to high-class cosmetics and masks.

Description

technical field [0001] The invention relates to the fields of biochemical industry and cosmetics, in particular to a preparation method of a natural antibacterial and water-retaining facial mask. Background technique [0002] At present, the beauty and skin care masks on the market are basically made of chemical synthetic fiber non-woven fabrics or artificial fiber non-woven fabrics through processes such as folding, bagging, injecting soaking liquid, and sealing, but synthetic fiber non-woven fabrics or artificial fiber Non-woven fabrics generally have degradation problems and cannot be recycled, and they are easy to cause environmental pollution after consumers use them. The fibers and adhesives of the non-woven fabric will partially dissolve under long-term immersion in the soaking solution, thus reducing the use effect of the mask and even causing allergies to consumers. In addition, the soaking solution of commonly used facial masks is thickened with polymer synthetic ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/144D06M16/00D06M10/02D01F8/12D04H1/728D01D5/00A61K8/02A61K8/88A61K8/34A61Q19/00D06M101/34
CPCA61K8/0212A61K8/342A61K8/88A61Q19/00D01D5/003D01F8/12D04H1/728D06M10/025D06M13/144D06M16/003D06M2101/34D06M2200/50
Inventor 汤佳鹏葛彦朱俐
Owner 广州黛香源生物科技有限公司
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