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Preparation method of aromatic, antibacterial and waterproof non-woven fabric

A non-woven fabric and aromatic technology, applied in textiles and papermaking, conjugated artificial filaments, conjugated synthetic polymer artificial filaments, etc., can solve problems such as swelling and disintegration, and achieve improved stability and antibacterial performance Effect

Active Publication Date: 2019-12-13
GUANGZHOU FOURTO SANITARY PRODUCTS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In particular, chitosan and polyethylene oxide have a certain degree of water solubility, which will swell and disintegrate after forming the material, which will also cause a burst release effect in the later stage of release.

Method used

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  • Preparation method of aromatic, antibacterial and waterproof non-woven fabric
  • Preparation method of aromatic, antibacterial and waterproof non-woven fabric
  • Preparation method of aromatic, antibacterial and waterproof non-woven fabric

Examples

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preparation example Construction

[0031] A method for preparing an aromatic antibacterial waterproof nonwoven fabric, comprising the steps of:

[0032] S1: Weigh the organic-inorganic composite lipid and antibacterial agent with a mass ratio of (0.1-0.2):(1-3), dissolve the organic-inorganic composite lipid in chloroform, evaporate and remove the chloroform To obtain a lipid-like film, add an antibacterial agent to the lipid-like film, stir and mix evenly, and rapidly heat to 45-50°C, maintain it for 10-30s while performing ultrasound in a water bath, then cool to 4°C and let it stand still. Extrude through a liposome extruder to obtain an antibacterial siliceous solution;

[0033] S2: Dissolving chitosan and polyethylene oxide completely in 90v / v% acetic acid solution, stirring evenly, to obtain spinning solution;

[0034] S3: using the spinning solution to perform electrospinning to obtain chitosan / polyethylene oxide nanofibers;

[0035] S4: immersing the nanofibers obtained in step S3 into the antibacteri...

Embodiment 1

[0052] A method for preparing an aromatic antibacterial waterproof nonwoven fabric, comprising the steps of:

[0053] 1. Preparation of organic-inorganic composite lipid: Dissolve 15g of N,N-bis(octadecylpropylamino)glycine in 100ml of triethylamine, then add 15g of aminopropyltriethoxysilane, and add at 0°C 6g of condensation reagent benzotriazol-1-yl-oxytripyrrolidinyl phosphonium hexafluorophosphate (PyBOP) was reacted for 6h, and after the reaction was completed, the organic-inorganic composite lipid was collected by silica gel column chromatography;

[0054] 2. Preparation of antibacterial siliceous body: Weigh 0.15g organic-inorganic composite lipid, dissolve organic-inorganic composite lipid in 10ml chloroform, remove chloroform by evaporation to obtain lipid-like film; dissolve 100ml 30g / L Add the tea tree essential oil solution into the obtained lipid film, stir and mix well, and rapidly heat up to 50°C, heat shock for 20s while ultrasonically in a water bath, cool to...

Embodiment 2

[0061] A method for preparing an aromatic antibacterial waterproof nonwoven fabric, comprising the steps of:

[0062] 1. Preparation of organic-inorganic composite lipid: Dissolve 10g of N,N-bis(octadecylpropylamino)glycine in 100ml of pyridine, then add 10g of aminopropyltriethoxysilane, and add 4g of it at -10°C The condensation reagent dicyclohexylcarbodiimide (DCC) was reacted for 4 hours, and after the reaction was completed, the organic-inorganic composite lipid was collected by silica gel column chromatography;

[0063] 2. Preparation of antibacterial siliceous body: Weigh 0.1g organic-inorganic composite lipid, dissolve organic-inorganic composite lipid in 10ml chloroform, remove chloroform by evaporation to obtain lipid-like film; dissolve 150ml 20g / L Add the eucalyptus essential oil solution into the obtained lipid film, stir and mix well, then heat rapidly to 45°C, heat shock for 10s while ultrasonically in a water bath, cool to 4°C, let stand, and extrude through p...

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Abstract

The invention discloses a preparation method of an aromatic, antibacterial and waterproof non-woven fabric and belongs to the field of textile engineering. The provided preparation method comprises the steps of (1) wrapping an antibacterial agent in a stable siliceous body formed by organic and inorganic composite lipid; (2) completely dissolving a certain amount of chitosan and polyethylene oxidein a 90% acetic acid solution, and uniformly stirring the mixture to obtain a spinning solution; (3) adopting the spinning solution for carrying out electrostatic spinning to obtain a chitosan / polyethylene oxide nanofiber; (4) soaking the nanofiber in an antibacterial siliceous body solution for a grafting reaction, treating the nanofiber by a plasma processor, and then air-drying the nanofiber;(5) soaking the air-dried nanofiber in an ethanol solution containing organic and inorganic composite lipid, carrying out negative-pressure flash explosion, washing the nanofiber with water, and performing drying at the high temperature to obtain the aromatic, antibacterial and waterproof non-woven fabric. The non-woven fabric has the advantages of lasting antibacterial effect, good waterproof performance and certain plant fragrance.

Description

technical field [0001] The invention relates to the field of textile engineering, in particular to a method for preparing an aromatic antibacterial and waterproof nonwoven fabric. Background technique [0002] When traditional non-woven fabrics, cotton yarns and other materials are used as medical fabrics, due to the thicker fabric fiber diameter and larger fiber pore size, the filtering effect on particles carrying pathogenic bacteria is not ideal. However, nanofibers are used as medical fabrics, and their ultra-fine diameter and extremely small porosity can effectively filter substances such as disease-bearing particles. However, as antibacterial nanofibers, if the antibacterial agent and high polymer are simply electrostatically blended, the phenomenon of burst release of antibacterial drugs will inevitably occur. [0003] In addition, due to the loose surface of the non-woven fabric, its water-permeable and water-conducting properties are better, and vice versa, its wat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M13/513D06M10/02D06M10/08D01F8/18D01F8/16D06M101/30
CPCD06M13/513D06M10/025D06M10/08D06M16/00D01F8/18D01F8/16D06M2101/30
Inventor 葛彦
Owner GUANGZHOU FOURTO SANITARY PRODUCTS CO LTD
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