Preparation method of efficient condensation hydrophilic and hydrophobic thin-film coating with multi-scale structure
A hydrophilic-hydrophobic, multi-scale technology, applied in the direction of coating, etc., can solve the problem that the condensation performance of the super-hydrophobic wall surface is difficult to further improve, and achieve the effects of improving condensation efficiency, low reaction temperature, and low energy consumption
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[0043] The invention provides a preparation method of a high-efficiency condensation hydrophilic and hydrophobic film coating with multi-scale structure, such as figure 1 shown, including:
[0044] Step 101, preparing a titanium dioxide film with a micron and nanometer secondary composite structure on a glass substrate;
[0045] Step 102, modifying the titanium dioxide film;
[0046] In step 103, a combined hydrophilic and hydrophobic surface is prepared by using an ultraviolet mask photolithography method.
Embodiment
[0049] Step 1: Preparation of TiO2 Thin Films with Micro- and Nano-Secondary Composite Structures
[0050] First, the surface of the glass substrate is treated by a plasma cleaner, and the cleaned glass sheet is placed in a solution of concentrated sulfuric acid: hydrogen peroxide solution = 7:3 (volume ratio), kept in a vacuum drying box at 80 °C for 2 hours, and high-purity water is used. Rinse, place it in an ultrasonic cleaner for 15 minutes, rinse with high-purity water, and finally dry it with high-purity nitrogen for use.
[0051] Put 1 mol / L titanium trichloride solution and add an appropriate amount of sodium chloride and pre-treated glass sheets together into a reaction kettle containing a polytetrafluoroethylene lining (a custom-made bracket is set in the lining, and glass sheets are added. stability in the reactor), uniformly heated from 90°C to 160°C, heating rate of about 1.2°C / min, kept at 160°C for 2 hours, cooled to room temperature, taken out, rinsed slowly w...
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Abstract
Description
Claims
Application Information
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