A kind of extraction method of active ingredient in ginger
The technology of an active ingredient and an extraction method is applied in the field of extraction of active ingredients in ginger, can solve the problems of waste of resources, effective separation, poor use effect, etc., and achieves the effects of avoiding waste, easy extraction, and improving extraction rate
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Embodiment 1
[0032] The present embodiment provides a kind of extracting method of active ingredient in ginger, a kind of extracting method of active ingredient in ginger, comprises the following steps:
[0033] (1) Ginger juice and minced ginger are obtained after the dried ginger is pulverized by an extrusion crushing device;
[0034] (2) Mix ginger juice and ginger powder, mix according to the ratio of 1g ginger to 8ml60% ethanol, and divide them into 3 groups, ultrasonic treatment for 13min, 15min, 20min respectively, and then carry out the above steps again on the centrifuged filter residue treatment, and then centrifuged to obtain the second filtrate and filter residue A, and the filtrate obtained by the first extraction and the second filtrate were combined to obtain filtrate A, wherein the treatment temperature was 50°C, the ultrasonic working power was 350W, and the centrifugal speed was 3600r / min. The time is 15 minutes;
[0035] (3) Filtrate A is mixed with an equal volume of p...
Embodiment 2
[0042] The present embodiment provides a kind of extracting method of active ingredient in ginger, a kind of extracting method of active ingredient in ginger, comprises the following steps:
[0043] (1) Ginger juice and minced ginger are obtained after the dried ginger is pulverized by an extrusion crushing device;
[0044] (2) Mix ginger juice and minced ginger, divide them into 3 groups, and mix them with 60% ethanol respectively, and the mixing ratios are 1:4, 1:5, 1:9, and divide them into 3 groups. Ultrasonic treatment for 15min, then the filter residue obtained by centrifugation was processed in the above steps again, and then centrifuged to obtain the second filtrate and filter residue A, and the filtrate obtained by the first extraction was combined with the second filtrate to obtain filtrate A, wherein the processing temperature was 50 ℃, the ultrasonic working power is 300W, the centrifugal speed is 3600r / min, and the centrifugal time is 15min;
[0045] (3) Filtrate...
Embodiment 3
[0052] Ginger essential oil and gingerol crude product are extracted according to the method among the embodiment 2, wherein in step (2), set and only carry out the control group of processing once with ultrasonic wave and process 3 times with ultrasonic wave, the ginger essential oil that it makes and gingerol extraction rate as shown in table 3:
[0053] table 3
[0054]
[0055] It can be seen from the above table that the extraction rate of active ingredients in the second extraction with ethanol is obviously higher than that in the first extraction with ethanol, while the extraction rate of active ingredients in the third extraction with ethanol is similar to the extraction rate of the active ingredients in the second extraction with ethanol, that is, using One-time ethanol extraction cannot effectively extract the active ingredients in ginger, and the second extraction can more thoroughly extract the active ingredients in ginger.
[0056] Wherein, the extrusion crush...
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