A kind of bridging plugging slurry and preparation method thereof
A technology for slurry leakage and asphalt layer, which is applied in the directions of chemical instruments and methods, drilling composition, etc., can solve the problem that leakage plugging slurry and asphalt channeling can not be effectively solved, and is not suitable for asphalt layer plugging, and the viscosity of leakage plugging slurry can not be effectively solved. It can improve the plugging effect, reduce the complexity and ensure the safety of drilling.
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preparation example Construction
[0042] The preparation method of the gel adopts the method of Example 8 in the Chinese patent publication CN106317321A, specifically comprising the following steps:
[0043] Add 17g of acrylamide, 4g of acryloyloxyethyltrimethylammonium chloride, and 0.2g of N,N'-methylenebisacrylamide into 100g of water, stir to fully dissolve, add 4g of ammonium alginate, stir to fully dissolve, add 0.5g of superfine calcium carbonate, stir to fully disperse, add 1g of ammonium persulfate and 1g of acetic acid, stir to dissolve fully, finally, place the mixed system at 55°C for reaction, and form a gel after 2 hours.
Embodiment 1
[0045] Formula: (unit is weight part)
[0046] Water: 100
[0047] Gels: 1
[0048] Calcium carbonate particles (1mm): 5
[0049] Walnut shell (0.5-1mm): 2
[0050] Suspension polymerization monoene-diene cross-linked gel resin (1mm): 0.5
[0051] Sepiolite fiber (0.5-1mm): 2
[0052] Mica (0.5mm): 2
[0053] Calcium carbonate powder (400 mesh): 5
[0054] Preparation method: Mix the gel with water to make a gel solution, add the above-mentioned other materials into the gel solution, stir at 4500r / min for 10min, prepare 1000mL gel plugging slurry according to the above formula, and set aside.
[0055] Test method: install a 1mm simulated fracture core in the DL-2 plugging instrument, fill the core fracture with 190g of asphalt, then add 1000mL gel plugging slurry and 1000mL drilling fluid into the DL-2 plugging instrument, and replace it with drilling fluid Gel plugging slurry. The core with simulated fractures was heated to 120°C and pressurized slowly. During the proce...
Embodiment 2
[0057] Formula: (unit is weight part)
[0058] Water: 100
[0059] Gels: 1
[0060] Clam shell powder (2mm): 6
[0061] Apricot shell (0.5-2mm): 2
[0062] EPDM and 4-tert-butylstyrene copolymer (1mm): 2
[0063] Aluminum silicate fiber (0.5-1mm): 2
[0064] Raw vermiculite (0.5mm): 2
[0065] Calcium sulfate powder (400 mesh): 5
[0066] Preparation method: mix the gel with water to make a gel solution, add other materials into the gel solution respectively, stir at 4500r / min for 10min, prepare 1000mL gel plugging slurry according to the above formula, and set aside.
[0067] Test method: install a 2mm simulated fracture core in the DL-2 plugging instrument, fill the core fracture with 380g of asphalt, then add 1000mL gel plugging slurry and 1000mL drilling fluid into the DL-2 plugging instrument, and replace it with drilling fluid Gel plugging slurry. The simulated fractured core was heated to 120°C and slowly pressurized. During the pressurization process, the aspha...
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